[(3aR,5S,6R,6aR)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl]-methanol

Base Information

Chemical Name:[(3aR,5S,6R,6aR)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl]-methanol
CAS No.:75772-03-1
Molecular Formula:C₂₅H₃₄O₅Si
Molecular Weight:442.627
Hs Code.:

Synonyms:[(3aR,5S,6R,6aR)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl]-methanol

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Chemical Property of [(3aR,5S,6R,6aR)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl]-methanol

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Technology Process of [(3aR,5S,6R,6aR)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl]-methanol

There total 8 articles about [(3aR,5S,6R,6aR)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl]-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75783-45-8
(3aR,5R,6aS)-5-[[(tert-butyldiphenylsilyl)oxy]methyl]-2,2-dimethyltetrahydro-2H-furo[2,3-d][1,3]dioxol-6-one

: 75772-03-1
[(3aR,5S,6R,6aR)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl]-methanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi

2.1: BH₃

2.2: 78 percent / H₂O₂

With n-butyllithium; borane; 1.1: Wittig reaction;
DOI:10.1081/NCN-100002355

Reference yield:

: 20031-21-4
1,2-O-isopropylidene-α-D-xylose

: 75772-03-1
[(3aR,5S,6R,6aR)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl]-methanol

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridinium dichromate / acetic anhydride

2.1: n-BuLi

3.1: BH₃

3.2: 78 percent / H₂O₂

With dipyridinium dichromate; n-butyllithium; borane; In acetic anhydride; 3.1: Wittig reaction;
DOI:10.1081/NCN-100002355

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 75772-03-1
[(3aR,5S,6R,6aR)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl]-methanol

Guidance literature:: Multi-step reaction with 3 steps

2: BuLi / 1,2-dimethoxy-ethane

3: H₂ / Pd-C / ethanol

With n-butyllithium; hydrogen; palladium on activated charcoal; In 1,2-dimethoxyethane; ethanol;
DOI:10.1039/c39800000556