O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-benzoyl-β-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-N-(benzyl N-benzyloxycarbonyl)-L-β-aspartyl-α-D-glucopyranosylamine

Base Information

Chemical Name:O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-benzoyl-β-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-N-(benzyl N-benzyloxycarbonyl)-L-β-aspartyl-α-D-glucopyranosylamine
CAS No.:127594-31-4
Molecular Formula:C₁₀₇H₁₀₄N₂O₂₃
Molecular Weight:1786
Hs Code.:

O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-benzoyl-β-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-N-(benzyl N-benzyloxycarbonyl)-L-β-aspartyl-α-D-glucopyranosylamine

Synonyms:O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-benzoyl-β-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-N-(benzyl N-benzyloxycarbonyl)-L-β-aspartyl-α-D-glucopyranosylamine

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Chemical Property of O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-benzoyl-β-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-N-(benzyl N-benzyloxycarbonyl)-L-β-aspartyl-α-D-glucopyranosylamine

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Technology Process of O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-benzoyl-β-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-N-(benzyl N-benzyloxycarbonyl)-L-β-aspartyl-α-D-glucopyranosylamine

There total 2 articles about O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-benzoyl-β-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-N-(benzyl N-benzyloxycarbonyl)-L-β-aspartyl-α-D-glucopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 127570-61-0
2,3,4-tri-O-benzyl-N-(benzyl N-benzyloxycarbonyl-L-β-aspartyl)-α-D-glucopyranosylamine

: C₆₆H₆₆O₁₄

: 127594-31-4
O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-benzoyl-β-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-N-(benzyl N-benzyloxycarbonyl)-L-β-aspartyl-α-D-glucopyranosylamine

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; In dichloromethane;
DOI:10.1021/ja00170a055

Reference yield:

: 127570-61-0
2,3,4-tri-O-benzyl-N-(benzyl N-benzyloxycarbonyl-L-β-aspartyl)-α-D-glucopyranosylamine

: 127594-30-3
pent-4-enyl 2,3,4-tri-O-benzoyl-6-O-(2,3,4,5-tetra-O-benzyl-α-D-glucopyranosyl)-α-D-glucopyranoside

: 127594-31-4
O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-benzoyl-β-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-N-(benzyl N-benzyloxycarbonyl)-L-β-aspartyl-α-D-glucopyranosylamine

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; Yield given. Multistep reaction; 1) CH₂Cl₂, r.t., 0.5 h;
DOI:10.1016/0008-6215(92)84171-N