Benzyl-3-O-(4-O-acetyl-2,6-didesoxy-2-iod-3-C-methyl-α-L-mannopyranosyl)-4-O-benzyl-2,6-didesoxy-α-D-arabino-hexopyranosid

Base Information

Chemical Name:Benzyl-3-O-(4-O-acetyl-2,6-didesoxy-2-iod-3-C-methyl-α-L-mannopyranosyl)-4-O-benzyl-2,6-didesoxy-α-D-arabino-hexopyranosid
CAS No.:75810-08-1
Molecular Formula:C₂₉H₃₇IO₈
Molecular Weight:640.512
Hs Code.:

Synonyms:Benzyl-3-O-(4-O-acetyl-2,6-didesoxy-2-iod-3-C-methyl-α-L-mannopyranosyl)-4-O-benzyl-2,6-didesoxy-α-D-arabino-hexopyranosid

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Chemical Property of Benzyl-3-O-(4-O-acetyl-2,6-didesoxy-2-iod-3-C-methyl-α-L-mannopyranosyl)-4-O-benzyl-2,6-didesoxy-α-D-arabino-hexopyranosid

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Technology Process of Benzyl-3-O-(4-O-acetyl-2,6-didesoxy-2-iod-3-C-methyl-α-L-mannopyranosyl)-4-O-benzyl-2,6-didesoxy-α-D-arabino-hexopyranosid

There total 3 articles about Benzyl-3-O-(4-O-acetyl-2,6-didesoxy-2-iod-3-C-methyl-α-L-mannopyranosyl)-4-O-benzyl-2,6-didesoxy-α-D-arabino-hexopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 94902-25-7
4-O-acetyl-L-olivomycal

: 75124-38-8
Benzyl 4-O-Benzyl-2,6-dideoxy-α-D-arabino-hexopyranoside

: 75810-08-1
Benzyl-3-O-(4-O-acetyl-2,6-didesoxy-2-iod-3-C-methyl-α-L-mannopyranosyl)-4-O-benzyl-2,6-didesoxy-α-D-arabino-hexopyranosid

Guidance literature:: With N-iodo-succinimide; In acetonitrile; for 4h; Ambient temperature;
DOI:10.1002/cber.19801130919

Reference yield:

: 94902-25-7
4-O-acetyl-L-olivomycal

: 75810-08-1
Benzyl-3-O-(4-O-acetyl-2,6-didesoxy-2-iod-3-C-methyl-α-L-mannopyranosyl)-4-O-benzyl-2,6-didesoxy-α-D-arabino-hexopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: 13 percent / N-iodosuccinimide / acetonitrile / 12 h / 5 °C

2: 12 percent / NiCl₂ * 6 H₂O, NaBH₄ / methanol / 0.17 h

3: 54 percent / N-iodosuccinimide / acetonitrile / 4 h / Ambient temperature

With sodium tetrahydroborate; N-iodo-succinimide; nickel dichloride; In methanol; acetonitrile;
DOI:10.1002/cber.19801130919

Reference yield:

: 75810-04-7
Benzyl-3-O-(4-O-acetyl-2,6-didesoxy-2-iod-3-C-methyl-α-L-mannopyranosyl)-4-O-benzyl-2,6-didesoxy-6-iod-α-D-arabino-hexopyranosid

: 75810-08-1
Benzyl-3-O-(4-O-acetyl-2,6-didesoxy-2-iod-3-C-methyl-α-L-mannopyranosyl)-4-O-benzyl-2,6-didesoxy-α-D-arabino-hexopyranosid

Guidance literature:: Multi-step reaction with 2 steps

1: 12 percent / NiCl₂ * 6 H₂O, NaBH₄ / methanol / 0.17 h

2: 54 percent / N-iodosuccinimide / acetonitrile / 4 h / Ambient temperature

With sodium tetrahydroborate; N-iodo-succinimide; nickel dichloride; In methanol; acetonitrile;
DOI:10.1002/cber.19801130919