2,3-diphenyl-1,4-benzodithiin

Base Information

Chemical Name:2,3-diphenyl-1,4-benzodithiin
CAS No.:55625-74-6
Molecular Formula:C₂₀H₁₄S₂
Molecular Weight:318.463
Hs Code.:

Synonyms:2,3-diphenyl-1,4-benzodithiin

Suppliers and Price of 2,3-diphenyl-1,4-benzodithiin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2,3-diphenyl-1,4-benzodithiin

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of 2,3-diphenyl-1,4-benzodithiin

There total 4 articles about 2,3-diphenyl-1,4-benzodithiin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 501-65-5
diphenyl acetylene

: 304915-28-4
1-(4-methylbenzylsulfinyl)-2-(4-methylbenzylthio)benzene

: 55625-74-6
2,3-diphenyl-1,4-benzodithiin

Guidance literature:: 1-(4-methylbenzylsulfinyl)-2-(4-methylbenzylthio)benzene; With trifluoromethylsulfonic anhydride; In dichloromethane; acetonitrile; at -60 ℃; for 0.00833333h;

diphenyl acetylene; In dichloromethane; acetonitrile; at -60 - 20 ℃; for 1.16667h; Further stages.;
DOI:10.1039/b004940i

Reference yield:

: 17534-15-5
Benzene-1,2-dithiol

: 55625-74-6
2,3-diphenyl-1,4-benzodithiin

Guidance literature:: Multi-step reaction with 3 steps

1.1: 86 percent / KOH

2.1: 73 percent / MCPBA

3.1: Tf₂O / acetonitrile; CH₂Cl₂ / 0.01 h / -60 °C

3.2: 44 percent / acetonitrile; CH₂Cl₂ / 1.17 h / -60 - 20 °C

With potassium hydroxide; trifluoromethylsulfonic anhydride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetonitrile; 1.1: Alkylation / 2.1: Oxidation / 3.1: Dealkylation / 3.2: Cycloaddition;
DOI:10.1039/b004940i

Reference yield:

: 304915-29-5
1,2-bis(4-methylbenzylthio)benzene

: 55625-74-6
2,3-diphenyl-1,4-benzodithiin

Guidance literature:: Multi-step reaction with 2 steps

1.1: 73 percent / MCPBA

2.1: Tf₂O / acetonitrile; CH₂Cl₂ / 0.01 h / -60 °C

2.2: 44 percent / acetonitrile; CH₂Cl₂ / 1.17 h / -60 - 20 °C

With trifluoromethylsulfonic anhydride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetonitrile; 1.1: Oxidation / 2.1: Dealkylation / 2.2: Cycloaddition;
DOI:10.1039/b004940i