5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalic acid 1-[2-(tert-butyloxycarbonyl)ethyl]amide

Base Information

Chemical Name:5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalic acid 1-[2-(tert-butyloxycarbonyl)ethyl]amide
CAS No.:1146730-44-0
Molecular Formula:C₄₁H₄₉N₅O₁₁
Molecular Weight:787.867
Hs Code.:

5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalic acid 1-[2-(tert-butyloxycarbonyl)ethyl]amide

Synonyms:5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalic acid 1-[2-(tert-butyloxycarbonyl)ethyl]amide

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Chemical Property of 5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalic acid 1-[2-(tert-butyloxycarbonyl)ethyl]amide

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Technology Process of 5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalic acid 1-[2-(tert-butyloxycarbonyl)ethyl]amide

There total 1 articles about 5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalic acid 1-[2-(tert-butyloxycarbonyl)ethyl]amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1146730-42-8
5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalic acid 1-[2-(tert-butyloxycarbonyl)ethyl]amide 4-methyl ester

: 1146730-44-0
5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalic acid 1-[2-(tert-butyloxycarbonyl)ethyl]amide

Guidance literature:: With potassium carbonate; In ethanol; water; at 50 ℃; for 2h;
DOI:10.1002/chem.200802151

Reference yield:

: 1146730-44-0
5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalic acid 1-[2-(tert-butyloxycarbonyl)ethyl]amide

: 58620-93-2
tert-butyl 3-aminopropanoate hydrochloride

: 1146730-46-2
5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalic acid 1,4-bis[2-(tert-butyloxycarbonyl)ethyl]amide

Guidance literature:: 5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalic acid 1-[2-(tert-butyloxycarbonyl)ethyl]amide; With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 0.0166667h;

tert-butyl 3-aminopropanoate hydrochloride; With benzotriazol-1-ol; triethylamine; In dichloromethane; at 80 ℃; for 48h;
DOI:10.1002/chem.200802151