C₃₇H₄₈N₂O₇

Base Information

• Chemical Name: C₃₇H₄₈N₂O₇
• CAS No.: 1343505-30-5
• Molecular Formula: C₃₇H₄₈N₂O₇
• Molecular Weight: 632.797
• Mol file: 1343505-30-5.mol

Synonyms:C₃₇H₄₈N₂O₇

Chemical Property of C₃₇H₄₈N₂O₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₇H₄₈N₂O₇

There total 9 articles about C₃₇H₄₈N₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

C40H52N2O7 (1343505-27-0) → C37H48N2O7 (1343505-30-5)

Guidance literature:

With morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 20 ℃;

DOI:10.1016/j.tetlet.2011.08.158

Reference yield:

C18H30O4 (1343505-09-8) → C37H48N2O7 (1343505-30-5)

Guidance literature:

Multi-step reaction with 8 steps

1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 2 h / -10 °C / Molecular sieve

2: 2,6-dimethylpyridine / dichloromethane / 0.75 h / 20 °C

3: diisobutylaluminium hydride / dichloromethane / 2 h / -40 - -10 °C

4: Dess-Martin periodane / dichloromethane / 1 h / 0 - 20 °C

5: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 1 h

6: 1-ethyl-piperidine; HATU / acetonitrile / 12 h / 0 - 20 °C

7: CSA / methanol; dichloromethane / 1 h / 0 °C

8: morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 20 °C

With morpholine; 1-ethyl-piperidine; 2,6-dimethylpyridine; sodium chlorite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; diisobutylaluminium hydride; Dess-Martin periodane; HATU; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile; tert-butyl alcohol;

DOI:10.1016/j.tetlet.2011.08.158

Reference yield:

C18H28O4 (1343505-16-7) → C37H48N2O7 (1343505-30-5)

Guidance literature:

Multi-step reaction with 7 steps

1: 2,6-dimethylpyridine / dichloromethane / 0.75 h / 20 °C

2: diisobutylaluminium hydride / dichloromethane / 2 h / -40 - -10 °C

3: Dess-Martin periodane / dichloromethane / 1 h / 0 - 20 °C

4: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 1 h

5: 1-ethyl-piperidine; HATU / acetonitrile / 12 h / 0 - 20 °C

6: CSA / methanol; dichloromethane / 1 h / 0 °C

7: morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 20 °C

With morpholine; 1-ethyl-piperidine; 2,6-dimethylpyridine; sodium chlorite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; diisobutylaluminium hydride; Dess-Martin periodane; HATU; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile; tert-butyl alcohol;

DOI:10.1016/j.tetlet.2011.08.158

upstream raw materials:

C₁₈H₃₀O₄

C₁₈H₂₈O₄

C₂₄H₄₂O₄Si

C₂₄H₄₄O₄Si