3-(3,5-di-O-acetyl-2-deoxy-β-D-erythro-pentofuranosyl)-6-[(4-propylphenyl)ethynyl]furo[2,3-d]pyrimidin-2(3H)-one

Base Information

• Chemical Name: 3-(3,5-di-O-acetyl-2-deoxy-β-D-erythro-pentofuranosyl)-6-[(4-propylphenyl)ethynyl]furo[2,3-d]pyrimidin-2(3H)-one
• CAS No.: 948559-77-1
• Molecular Formula: C₂₆H₂₆N₂O₇
• Molecular Weight: 478.502

Synonyms:3-(3,5-di-O-acetyl-2-deoxy-β-D-erythro-pentofuranosyl)-6-[(4-propylphenyl)ethynyl]furo[2,3-d]pyrimidin-2(3H)-one

Chemical Property of 3-(3,5-di-O-acetyl-2-deoxy-β-D-erythro-pentofuranosyl)-6-[(4-propylphenyl)ethynyl]furo[2,3-d]pyrimidin-2(3H)-one

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Technology Process of 3-(3,5-di-O-acetyl-2-deoxy-β-D-erythro-pentofuranosyl)-6-[(4-propylphenyl)ethynyl]furo[2,3-d]pyrimidin-2(3H)-one

There total 1 articles about 3-(3,5-di-O-acetyl-2-deoxy-β-D-erythro-pentofuranosyl)-6-[(4-propylphenyl)ethynyl]furo[2,3-d]pyrimidin-2(3H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

6-bromo-3-(3,5-di-O-acetyl-2-deoxy-β-D-erythro-pentofuranosyl)-furo[2,3-d]pyrimidin-2(3H)-one (873325-86-1) + 1-ethynyl-4-propylbenzene (62452-73-7) → 3-(3,5-di-O-acetyl-2-deoxy-β-D-erythro-pentofuranosyl)-6-[(4-propylphenyl)ethynyl]furo[2,3-d]pyrimidin-2(3H)-one (948559-77-1)

Guidance literature:

With triethylamine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; for 3h;

DOI:10.1021/jm070210n

Reference yield: 63.0%

3-(3,5-di-O-acetyl-2-deoxy-β-D-erythro-pentofuranosyl)-6-[(4-propylphenyl)ethynyl]furo[2,3-d]pyrimidin-2(3H)-one (948559-77-1) → 3-(3,5-di-O-acetyl-2-deoxy-β-D-erythro-pentofuranosyl)-6-[(4-propylphenyl)ethyl]furo[2,3-d]pyrimidin-2(3H)-one (948559-88-4)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; at 20 ℃; for 5h; under 1292.9 Torr;

DOI:10.1021/jm070210n

Reference yield: 47.0%

3-(3,5-di-O-acetyl-2-deoxy-β-D-erythro-pentofuranosyl)-6-[(4-propylphenyl)ethynyl]furo[2,3-d]pyrimidin-2(3H)-one (948559-77-1) → C22H22N2O5

Guidance literature:

With ammonia; In methanol; at 0 ℃; for 3h;

DOI:10.1021/jm070210n

upstream raw materials:

6-bromo-3-(3,5-di-O-acetyl-2-deoxy-β-D-erythro-pentofuranosyl)-furo[2,3-d]pyrimidin-2(3H)-one

1-ethynyl-4-propylbenzene

Downstream raw materials:

3-(3,5-di-O-acetyl-2-deoxy-β-D-erythro-pentofuranosyl)-6-[(4-propylphenyl)ethyl]furo[2,3-d]pyrimidin-2(3H)-one

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