(2-Imino-1,2-dihydro-benzo[cd]indol-6-yl)-[4-(4-methoxy-benzenesulfonyl)-benzyl]-methyl-amine

Base Information

Chemical Name:(2-Imino-1,2-dihydro-benzo[cd]indol-6-yl)-[4-(4-methoxy-benzenesulfonyl)-benzyl]-methyl-amine
CAS No.:138384-69-7
Molecular Formula:C₂₆H₂₃N₃O₃S
Molecular Weight:457.553
Hs Code.:

Synonyms:(2-Imino-1,2-dihydro-benzo[cd]indol-6-yl)-[4-(4-methoxy-benzenesulfonyl)-benzyl]-methyl-amine

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Chemical Property of (2-Imino-1,2-dihydro-benzo[cd]indol-6-yl)-[4-(4-methoxy-benzenesulfonyl)-benzyl]-methyl-amine

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Technology Process of (2-Imino-1,2-dihydro-benzo[cd]indol-6-yl)-[4-(4-methoxy-benzenesulfonyl)-benzyl]-methyl-amine

There total 12 articles about (2-Imino-1,2-dihydro-benzo[cd]indol-6-yl)-[4-(4-methoxy-benzenesulfonyl)-benzyl]-methyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 130-00-7
1,8-naphtholactam

: 138384-69-7
(2-Imino-1,2-dihydro-benzo[cd]indol-6-yl)-[4-(4-methoxy-benzenesulfonyl)-benzyl]-methyl-amine

Guidance literature:: Multi-step reaction with 7 steps

1: 51 percent / 70percent HNO₃ / acetic acid / 1 h / 20 - 50 °C

2: H₂ / 5percent Pd/C / tetrahydrofuran / 16 h / 2068.6 Torr

3: DIEA / dimethylformamide

4: DIEA / dimethylformamide

5: Lawesson's reagent / toluene

6: NaOH / tetrahydrofuran; ethanol

7: NH₃ / methanol

With Lawessons reagent; sodium hydroxide; ammonia; hydrogen; nitric acid; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; acetic acid; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm00082a006

Reference yield:

: 28434-96-0
N-hydroxy-4-nitro-1,8-naphthalimide

: 138384-69-7
(2-Imino-1,2-dihydro-benzo[cd]indol-6-yl)-[4-(4-methoxy-benzenesulfonyl)-benzyl]-methyl-amine

Guidance literature:: Multi-step reaction with 8 steps

1: Na₂CO₃ / H₂O / 1 h / Heating

2: NaOH / ethanol; H₂O / 16 h / 25 °C

3: H₂ / 5percent Pd/C / tetrahydrofuran / 16 h / 2068.6 Torr

4: DIEA / dimethylformamide

5: DIEA / dimethylformamide

6: Lawesson's reagent / toluene

7: NaOH / tetrahydrofuran; ethanol

8: NH₃ / methanol

With Lawessons reagent; sodium hydroxide; ammonia; hydrogen; sodium carbonate; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm00082a006

Reference yield:

: 65300-66-5
N-(2,4-dinitrophenoxy)-4-nitronaphthalimide

: 138384-69-7
(2-Imino-1,2-dihydro-benzo[cd]indol-6-yl)-[4-(4-methoxy-benzenesulfonyl)-benzyl]-methyl-amine

Guidance literature:: Multi-step reaction with 7 steps

1: NaOH / ethanol; H₂O / 16 h / 25 °C

2: H₂ / 5percent Pd/C / tetrahydrofuran / 16 h / 2068.6 Torr

3: DIEA / dimethylformamide

4: DIEA / dimethylformamide

5: Lawesson's reagent / toluene

6: NaOH / tetrahydrofuran; ethanol

7: NH₃ / methanol

With Lawessons reagent; sodium hydroxide; ammonia; hydrogen; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm00082a006