1,6,9-tris(4-tert-butylphenoxy)-N-(2,6-diisopropyl-4-ethynylphenyl)-3,4-perylenedicarboximide

Base Information

Chemical Name:1,6,9-tris(4-tert-butylphenoxy)-N-(2,6-diisopropyl-4-ethynylphenyl)-3,4-perylenedicarboximide
CAS No.:468083-01-4
Molecular Formula:C₆₆H₆₃NO₅
Molecular Weight:950.23
Hs Code.:

Synonyms:1,6,9-tris(4-tert-butylphenoxy)-N-(2,6-diisopropyl-4-ethynylphenyl)-3,4-perylenedicarboximide

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Chemical Property of 1,6,9-tris(4-tert-butylphenoxy)-N-(2,6-diisopropyl-4-ethynylphenyl)-3,4-perylenedicarboximide

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Technology Process of 1,6,9-tris(4-tert-butylphenoxy)-N-(2,6-diisopropyl-4-ethynylphenyl)-3,4-perylenedicarboximide

There total 1 articles about 1,6,9-tris(4-tert-butylphenoxy)-N-(2,6-diisopropyl-4-ethynylphenyl)-3,4-perylenedicarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1,6,9-tris(4-tert-butylphenoxy)-N-[2,6-diisopropyl-4-[2-(triisopropylsilyl)ethynyl]phenyl]-3,4-perylenedicarboximide

: 468083-01-4
1,6,9-tris(4-tert-butylphenoxy)-N-(2,6-diisopropyl-4-ethynylphenyl)-3,4-perylenedicarboximide

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 0.5h;
DOI:10.1016/S0040-4020(03)00020-6

Reference yield: 83.0%

: 56990-02-4
3,5-dibromobenzaldehyde

: 468083-01-4
1,6,9-tris(4-tert-butylphenoxy)-N-(2,6-diisopropyl-4-ethynylphenyl)-3,4-perylenedicarboximide

: 468083-02-5
3,5-bis[2-[4-[1,6,9-tris(4-tert-butylphenoxy)perylene-3,4-dicarboximido]-3,5-diisopropylphenyl]ethynyl]benzaldehyde

Guidance literature:: With copper(l) iodide; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; triphenylphosphine; In triethylamine; toluene; at 50 ℃;
DOI:10.1016/S0040-4020(03)00020-6

Reference yield: 80.0%

: 468083-01-4
1,6,9-tris(4-tert-butylphenoxy)-N-(2,6-diisopropyl-4-ethynylphenyl)-3,4-perylenedicarboximide

: 5-bromo-10,15,20-trimesitylporphyrin

: 5-[(2-(4-(1,6,9-tris(4-tert-butylphenoxy)-3,4-perylenedicarboximido)-3,5-diisopropylphenyl)ethynyl)]-10,15,20-trimesitylporphyrin

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triethylamine; tris-(o-tolyl)phosphine; In toluene; at 60 ℃; for 3h; Schlenk technique;
DOI:10.1021/jp411629m