(2E,4Z)-5-Ethoxy-5-phenyl-2-(pyrrolidine-1-carbonyl)-3-pyrrolidin-1-yl-penta-2,4-dienenitrile

Base Information

Chemical Name:(2E,4Z)-5-Ethoxy-5-phenyl-2-(pyrrolidine-1-carbonyl)-3-pyrrolidin-1-yl-penta-2,4-dienenitrile
CAS No.:102610-10-6
Molecular Formula:C₂₂H₂₇N₃O₂
Molecular Weight:365.475
Hs Code.:

Synonyms:(2E,4Z)-5-Ethoxy-5-phenyl-2-(pyrrolidine-1-carbonyl)-3-pyrrolidin-1-yl-penta-2,4-dienenitrile

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Chemical Property of (2E,4Z)-5-Ethoxy-5-phenyl-2-(pyrrolidine-1-carbonyl)-3-pyrrolidin-1-yl-penta-2,4-dienenitrile

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Technology Process of (2E,4Z)-5-Ethoxy-5-phenyl-2-(pyrrolidine-1-carbonyl)-3-pyrrolidin-1-yl-penta-2,4-dienenitrile

There total 1 articles about (2E,4Z)-5-Ethoxy-5-phenyl-2-(pyrrolidine-1-carbonyl)-3-pyrrolidin-1-yl-penta-2,4-dienenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 614-16-4
Benzoylacetonitrile

: C₁₆H₂₂NOS⁽¹⁺⁾*BF₄^(1-)

: 102610-10-6
(2E,4Z)-5-Ethoxy-5-phenyl-2-(pyrrolidine-1-carbonyl)-3-pyrrolidin-1-yl-penta-2,4-dienenitrile

Guidance literature:: With triethylamine; In benzene;
DOI:10.1016/S0040-4039(00)98699-4

Reference yield:

: 102610-10-6
(2E,4Z)-5-Ethoxy-5-phenyl-2-(pyrrolidine-1-carbonyl)-3-pyrrolidin-1-yl-penta-2,4-dienenitrile

: 102610-18-4
6-Phenyl-2,4-di-pyrrolidin-1-yl-nicotinonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 1) (COCl)2, 2) AcOH, HClO₄

2: 60 percent / NH₃ / 2-methyl-propan-2-ol / 20 °C

With perchloric acid; oxalyl dichloride; ammonia; acetic acid; In tert-butyl alcohol;
DOI:10.1016/S0040-4039(00)98699-4