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C17H23FN4O5S

Base Information
  • Chemical Name:C17H23FN4O5S
  • CAS No.:1402742-23-7
  • Molecular Formula:C17H23FN4O5S
  • Molecular Weight:414.458
  • Hs Code.:
C<sub>17</sub>H<sub>23</sub>FN<sub>4</sub>O<sub>5</sub>S

Synonyms:C17H23FN4O5S

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Chemical Property of C17H23FN4O5S
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Technology Process of C17H23FN4O5S

There total 22 articles about C17H23FN4O5S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With hydrogen; palladium on activated charcoal; In methanol; at 25 ℃; for 16h; under 1292.9 Torr;
Guidance literature:
Multi-step reaction with 10 steps
1.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 - -30 °C
1.2: -78 - 25 °C
2.1: hydrogen / palladium hydrogenation catalyst / ethanol
3.1: diethoxyltriphenylphosphorane / toluene / 60 h / 45 °C
4.1: water; lithium hydroxide / tetrahydrofuran / 60 °C
4.2: 25 °C / pH 3
5.1: triethylamine; diphenyl phosphoryl azide / tetrahydrofuran / 24 h / 25 °C
5.2: 1.5 h / 80 °C
6.1: trifluoroacetic acid / 1,3-Dimethoxybenzene; chloroform / 18 h
7.1: 4 h / Reflux
7.2: 12 h / 25 °C
8.1: nitric acid; sulfuric acid / 1 h / -10 °C
8.2: 12 h / 30 °C
9.1: carbon dioxide; ammonia / water; methanol / 38 °C / Resolution of racemate
10.1: hydrogen / palladium on activated charcoal / methanol / 16 h / 25 °C / 1292.9 Torr
With carbon dioxide; sulfuric acid; diphenyl phosphoryl azide; diethoxyltriphenylphosphorane; ammonia; water; hydrogen; nitric acid; sodium hexamethyldisilazane; triethylamine; trifluoroacetic acid; lithium hydroxide; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; chloroform; water; toluene; 1,3-Dimethoxybenzene;
Guidance literature:
Multi-step reaction with 9 steps
1.1: hydrogen / palladium hydrogenation catalyst / ethanol
2.1: diethoxyltriphenylphosphorane / toluene / 60 h / 45 °C
3.1: water; lithium hydroxide / tetrahydrofuran / 60 °C
3.2: 25 °C / pH 3
4.1: triethylamine; diphenyl phosphoryl azide / tetrahydrofuran / 24 h / 25 °C
4.2: 1.5 h / 80 °C
5.1: trifluoroacetic acid / 1,3-Dimethoxybenzene; chloroform / 18 h
6.1: 4 h / Reflux
6.2: 12 h / 25 °C
7.1: nitric acid; sulfuric acid / 1 h / -10 °C
7.2: 12 h / 30 °C
8.1: carbon dioxide; ammonia / water; methanol / 38 °C / Resolution of racemate
9.1: hydrogen / palladium on activated charcoal / methanol / 16 h / 25 °C / 1292.9 Torr
With carbon dioxide; sulfuric acid; diphenyl phosphoryl azide; diethoxyltriphenylphosphorane; ammonia; water; hydrogen; nitric acid; triethylamine; trifluoroacetic acid; lithium hydroxide; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; chloroform; water; toluene; 1,3-Dimethoxybenzene;
upstream raw materials:

C28H32FNO6S

C29H34FNO7S

C22H28FNO7S

C22H26FNO6S

Downstream raw materials:

C18H19FN6O5S

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