N-Methyl-2-(triphenylsilyl)-2,3-butadienanilid

Base Information

• Chemical Name: N-Methyl-2-(triphenylsilyl)-2,3-butadienanilid
• CAS No.: 79139-19-8
• Molecular Formula: C₂₉H₂₅NOSi
• Molecular Weight: 431.609
• Mol file: 79139-19-8.mol

Synonyms:N-Methyl-2-(triphenylsilyl)-2,3-butadienanilid

Chemical Property of N-Methyl-2-(triphenylsilyl)-2,3-butadienanilid

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of N-Methyl-2-(triphenylsilyl)-2,3-butadienanilid

There total 4 articles about N-Methyl-2-(triphenylsilyl)-2,3-butadienanilid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

N-Methyl-N-(triphenylsilylethinyl)anilin (57694-92-5) → 2-Acetyl-3-(N-methylanilino)-2-cyclobuten-1-on (73000-88-1) + N-Methyl-2-(triphenylsilyl)acetanilid (79139-20-1) + N-Methyl-2-(triphenylsilyl)-2,3-butadienanilid (79139-19-8) + triphenylhydroxysilane (791-31-1)

Guidance literature:

With Ketene; In acetonitrile; for 0.666667h; Further byproducts given; Ambient temperature;

Reference yield: 26.0%

Ketene (463-51-4) + N-Methyl-N-(triphenylsilylethinyl)anilin (57694-92-5) → 2-Acetyl-3-(N-methylanilino)-2-cyclobuten-1-on (73000-88-1) + N-Methyl-2-(triphenylsilyl)-2,3-butadienanilid (79139-19-8) + 3-(N-Methylanilino)-2-<3-(triphenylsiloxy)-3-butenoyl>-2-cyclobuten-1-on (79139-21-2) + triphenylhydroxysilane (791-31-1)

Guidance literature:

In acetonitrile; for 0.666667h; Further byproducts given; Ambient temperature;

Reference yield: 15.0%

Ketene (463-51-4) + N-Methyl-N-(triphenylsilylethinyl)anilin (57694-92-5) → 2-Acetyl-3-(N-methylanilino)-2-cyclobuten-1-on (73000-88-1) + 3-(N-Methylanilino)-2-(triphenylsilyl)-2-cyclobuten-1-on (79139-22-3) + N-Methyl-2-(triphenylsilyl)-2,3-butadienanilid (79139-19-8) + triphenylhydroxysilane (791-31-1)

Guidance literature:

In acetonitrile; for 0.666667h; Further byproducts given; Ambient temperature;

upstream raw materials:

Ketene

N-Methyl-N-(triphenylsilylethinyl)anilin