(2R,5'S,5''S)-4,5'-Dibenzyl-5''-(2,2-dimethoxy-ethyl)-2,5''-diisopropyl-1,2,1',5',1'',5''-hexahydro-[2,3';5',3'']terpyrrole-3,4',4''-trione

Base Information

Chemical Name:(2R,5'S,5''S)-4,5'-Dibenzyl-5''-(2,2-dimethoxy-ethyl)-2,5''-diisopropyl-1,2,1',5',1'',5''-hexahydro-[2,3';5',3'']terpyrrole-3,4',4''-trione
CAS No.:312913-00-1
Molecular Formula:C₃₆H₄₃N₃O₅
Molecular Weight:597.755
Hs Code.:

Synonyms:(2R,5'S,5''S)-4,5'-Dibenzyl-5''-(2,2-dimethoxy-ethyl)-2,5''-diisopropyl-1,2,1',5',1'',5''-hexahydro-[2,3';5',3'']terpyrrole-3,4',4''-trione

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Chemical Property of (2R,5'S,5''S)-4,5'-Dibenzyl-5''-(2,2-dimethoxy-ethyl)-2,5''-diisopropyl-1,2,1',5',1'',5''-hexahydro-[2,3';5',3'']terpyrrole-3,4',4''-trione

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Technology Process of (2R,5'S,5''S)-4,5'-Dibenzyl-5''-(2,2-dimethoxy-ethyl)-2,5''-diisopropyl-1,2,1',5',1'',5''-hexahydro-[2,3';5',3'']terpyrrole-3,4',4''-trione

There total 9 articles about (2R,5'S,5''S)-4,5'-Dibenzyl-5''-(2,2-dimethoxy-ethyl)-2,5''-diisopropyl-1,2,1',5',1'',5''-hexahydro-[2,3';5',3'']terpyrrole-3,4',4''-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (S)-2-[2-((2R,5'S)-4,5'-Dibenzyl-2-isopropyl-3,4'-dioxo-2,3,4',5'-tetrahydro-1H,1'H-[2,3']bipyrrolyl-5'-yl)-eth-(E)-ylideneamino]-2-(2,2-dimethoxy-ethyl)-3-methyl-butyric acid methyl ester

: 312913-00-1
(2R,5'S,5''S)-4,5'-Dibenzyl-5''-(2,2-dimethoxy-ethyl)-2,5''-diisopropyl-1,2,1',5',1'',5''-hexahydro-[2,3';5',3'']terpyrrole-3,4',4''-trione

Guidance literature:: With potassium hexamethylsilazane; In tetrahydrofuran;
DOI:10.1021/ja002964w

Reference yield:

: 104-53-0
3-phenyl-propionaldehyde

: 312913-00-1
(2R,5'S,5''S)-4,5'-Dibenzyl-5''-(2,2-dimethoxy-ethyl)-2,5''-diisopropyl-1,2,1',5',1'',5''-hexahydro-[2,3';5',3'']terpyrrole-3,4',4''-trione

Guidance literature:: Multi-step reaction with 8 steps

1: benzene

2: KHMDS / tetrahydrofuran

3: 95 percent / aq. TsOH / tetrahydrofuran

4: benzene

5: KHMDS / tetrahydrofuran

6: 97 percent / 4N aq. HCl / tetrahydrofuran

7: benzene

8: KHMDS / tetrahydrofuran

With hydrogenchloride; potassium hexamethylsilazane; toluene-4-sulfonic acid; In tetrahydrofuran; benzene;
DOI:10.1021/ja002964w

Reference yield:

: 312912-96-2
(S)-2-Amino-2-(2,2-dimethoxy-ethyl)-3-methyl-butyric acid methyl ester

: 312913-00-1
(2R,5'S,5''S)-4,5'-Dibenzyl-5''-(2,2-dimethoxy-ethyl)-2,5''-diisopropyl-1,2,1',5',1'',5''-hexahydro-[2,3';5',3'']terpyrrole-3,4',4''-trione

Guidance literature:: Multi-step reaction with 8 steps

1: benzene

2: KHMDS / tetrahydrofuran

3: 95 percent / aq. TsOH / tetrahydrofuran

4: benzene

5: KHMDS / tetrahydrofuran

6: 97 percent / 4N aq. HCl / tetrahydrofuran

7: benzene

8: KHMDS / tetrahydrofuran

With hydrogenchloride; potassium hexamethylsilazane; toluene-4-sulfonic acid; In tetrahydrofuran; benzene;
DOI:10.1021/ja002964w