C₃₆H₄₇⁽³⁾HN₄O₇

Base Information

Chemical Name:C₃₆H₄₇⁽³⁾HN₄O₇
CAS No.:197631-11-1
Molecular Formula:C₃₆H₄₈N₄O₇
Molecular Weight:650.792
Hs Code.:

C<sub>36</sub>H<sub>47</sub><sup>(3)</sup>HN<sub>4</sub>O<sub>7</sub>

Synonyms:C₃₆H₄₇⁽³⁾HN₄O₇

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₆H₄₇⁽³⁾HN₄O₇

Chemical Property:

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Technology Process of C₃₆H₄₇⁽³⁾HN₄O₇

There total 17 articles about C₃₆H₄₇⁽³⁾HN₄O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (4R,5S)-5-[5-((5S,8S,11S,13aR)-5,8-Dibenzyl-4,7,10,13-tetraoxo-tetradecahydro-3a,6,9,12-tetraaza-cyclopentacyclododecen-11-yl)-pentyl]-2,2-dimethyl-[1,3]dioxolane-4-carbaldehyde

: 197631-11-1
C₃₆H₄₇⁽³⁾HN₄O₇

Guidance literature:: With <3H>NaBH4; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1021/ja9615841

Reference yield:

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 197631-11-1
C₃₆H₄₇⁽³⁾HN₄O₇

Guidance literature:: Multi-step reaction with 9 steps

1: 1.) N-methylmorpholine, 2.) 1-hydroxybenzotriazole, 3.) 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide

2: trifluoroacetic acid / CH₂Cl₂ / 1 h

3: 1.) N-methylmorpholine, 2.) 1-hydroxybenzotriazole, 3.) 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide

4: aq. LiOH / tetrahydrofuran; methanol / 2 h / Ambient temperature

5: H₂ / 10percent Pd/C / tetrahydrofuran / 13.5 h

6: 4-(dimethylamino)pyridine, benzotrazol-1-yloxytris(dimethylamino)phosphonium hexafluorophosphate / dimethylformamide / 96 h / 25 °C

7: 51 percent / Bu₄NF / tetrahydrofuran / 1 h / Ambient temperature

8: Dess-Martin periodinane / CH₂Cl₂ / 1 h

9: <3H>NaBH₄ / tetrahydrofuran / 1 h / 0 °C

With 4-methyl-morpholine; dmap; lithium hydroxide; <3H>NaBH4; tetrabutyl ammonium fluoride; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; benzotriazol-1-ol; Dess-Martin periodane; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja9615841

Reference yield:

: 50622-09-8
2,3-O-isopropylidene-L-threitol

: 197631-11-1
C₃₆H₄₇⁽³⁾HN₄O₇

Guidance literature:: Multi-step reaction with 13 steps

1: 1.) NaH / 1.) THF, RT, 45 min, 2.) THF, 3 h

2: 1.) (COCl)2, DMSO, 2.) Et₃N / 1.) CH₂Cl₂, -78 deg C, 5 min, 2.) CH₂Cl₂, RT, 1 h

3: 1.) nBuLi / 1.) THF, -23 deg C, 1 h, 2.) THF, a) -78 deg C, 30 min, b) 0 deg C, 45 min

4: 99 percent / H₂ / 10percent Pd/C / ethyl acetate / 6 h

5: 97 percent / PPh₃, CBr₄ / tetrahydrofuran / 0.5 h / Ambient temperature

6: 1.) Mg, 1,2-dibromoethane, 2.) CuBr*Me₂S / 1.) Et₂O, 160 min, 2.) THF, Et₂O, -23 deg C, 140 min

7: 1.) N-methylmorpholine, 2.) 1-hydroxybenzotriazole, 3.) 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide

8: aq. LiOH / tetrahydrofuran; methanol / 2 h / Ambient temperature

9: H₂ / 10percent Pd/C / tetrahydrofuran / 13.5 h

10: 4-(dimethylamino)pyridine, benzotrazol-1-yloxytris(dimethylamino)phosphonium hexafluorophosphate / dimethylformamide / 96 h / 25 °C

11: 51 percent / Bu₄NF / tetrahydrofuran / 1 h / Ambient temperature

12: Dess-Martin periodinane / CH₂Cl₂ / 1 h

13: <3H>NaBH₄ / tetrahydrofuran / 1 h / 0 °C

With 4-methyl-morpholine; dmap; lithium hydroxide; n-butyllithium; oxalyl dichloride; copper(I) bromide dimethylsulfide complex; carbon tetrabromide; <3H>NaBH4; tetrabutyl ammonium fluoride; hydrogen; sodium hydride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; benzotriazol-1-ol; Dess-Martin periodane; magnesium; dimethyl sulfoxide; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; ethylene dibromide; triethylamine; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/ja9615841