(2E,6E,10E)-5-(benzenesulfonyl)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraenyl phenyl sulfide

Base Information

• Chemical Name: (2E,6E,10E)-5-(benzenesulfonyl)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraenyl phenyl sulfide
• CAS No.: 1011506-00-5
• Molecular Formula: C₃₂H₄₂O₂S₂
• Molecular Weight: 522.816

Synonyms:(2E,6E,10E)-5-(benzenesulfonyl)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraenyl phenyl sulfide

Chemical Property of (2E,6E,10E)-5-(benzenesulfonyl)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraenyl phenyl sulfide

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Technology Process of (2E,6E,10E)-5-(benzenesulfonyl)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraenyl phenyl sulfide

There total 1 articles about (2E,6E,10E)-5-(benzenesulfonyl)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraenyl phenyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

(((2E,6E,10E)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraen-1-yl)sulfonyl)benzene (38818-91-6) + 4-bromo-3-methyl-2-butenyl phenyl sulfide (359010-59-6) → (2E,6E,10E)-5-(benzenesulfonyl)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraenyl phenyl sulfide (1011506-00-5)

Guidance literature:

(((2E,6E,10E)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraen-1-yl)sulfonyl)benzene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

4-bromo-3-methyl-2-butenyl phenyl sulfide; In tetrahydrofuran; hexane; at -78 ℃; for 1.5h; Further stages.;

DOI:10.1021/jo702303a

Reference yield: 92.0%

(2E,6E,10E)-5-(benzenesulfonyl)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraenyl phenyl sulfide (1011506-00-5) → (2E,6E,10E)-1,5-bis(benzenesulfonyl)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraene (1011506-20-9)

Guidance literature:

With LiNbMoO₆; dihydrogen peroxide; In methanol; benzene; for 11h; cooling;

DOI:10.1021/jo702303a

upstream raw materials:

(((2E,6E,10E)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraen-1-yl)sulfonyl)benzene

4-bromo-3-methyl-2-butenyl phenyl sulfide

Downstream raw materials:

(2E,6E,10E)-1,5-bis(benzenesulfonyl)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraene

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