diethyl (acetylamino)<<2-(diethoxyphosphinyl)phenyl>methyl>propanedioate

Base Information

Chemical Name:diethyl (acetylamino)<<2-(diethoxyphosphinyl)phenyl>methyl>propanedioate
CAS No.:117571-56-9
Molecular Formula:C₂₀H₃₀NO₈P
Molecular Weight:443.434
Hs Code.:

Synonyms:diethyl (acetylamino)<<2-(diethoxyphosphinyl)phenyl>methyl>propanedioate

Suppliers and Price of diethyl (acetylamino)<<2-(diethoxyphosphinyl)phenyl>methyl>propanedioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of diethyl (acetylamino)<<2-(diethoxyphosphinyl)phenyl>methyl>propanedioate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of diethyl (acetylamino)<<2-(diethoxyphosphinyl)phenyl>methyl>propanedioate

There total 3 articles about diethyl (acetylamino)<<2-(diethoxyphosphinyl)phenyl>methyl>propanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.4%

: 120667-45-0
diethyl (acetylamino)<(2-bromophenyl)methyl>propanedioate

: 762-04-9
phosphonic acid diethyl ester

: 117571-56-9
diethyl (acetylamino)<<2-(diethoxyphosphinyl)phenyl>methyl>propanedioate

Guidance literature:: With triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 90 ℃; for 24h;
DOI:10.1021/jm00127a030

Reference yield:

: 1068-90-2
2-acetylaminomalonic acid diethyl ester

: 117571-56-9
diethyl (acetylamino)<<2-(diethoxyphosphinyl)phenyl>methyl>propanedioate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaOEt / 1.) EtOH, 15 min, 2.) THF, RT, overnight

2: 30.4 percent / triethylamine / tetrakis(triphenylphosphine)palladium⁽⁰⁾ / toluene / 24 h / 90 °C

With sodium ethanolate; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene;
DOI:10.1021/jm00127a030

Reference yield:

: 3433-80-5
1-Bromo-2-bromomethyl-benzene

: 117571-56-9
diethyl (acetylamino)<<2-(diethoxyphosphinyl)phenyl>methyl>propanedioate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaOEt / 1.) EtOH, 15 min, 2.) THF, RT, overnight

2: 30.4 percent / triethylamine / tetrakis(triphenylphosphine)palladium⁽⁰⁾ / toluene / 24 h / 90 °C

With sodium ethanolate; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene;
DOI:10.1021/jm00127a030