Technology Process of 9-bromononanoic acid allyl ester
There total 1 articles about 9-bromononanoic acid allyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 67 percent / Jones' reagent / acetone; H2O / 0 °C
2: 92 percent / p-TsOH / toluene / Heating
With
jones' reagent; toluene-4-sulfonic acid;
In
water; acetone; toluene;
DOI:10.1021/ol0613463
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 68 percent / AgNO2 / diethyl ether / 168 h / 20 °C
2: 81 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / 20 °C
3: 86 percent / p-toluenesulfonic acid / 20 °C
4: 84 percent / Na2CO3 / benzene / 24 h / 80 - 90 °C
5: 95 percent / formic acid; Pd(PPh3)4 / tetrahydrofuran / 24 h / Heating
6: ethanol / 1 h / 20 °C
With
tetrakis(triphenylphosphine) palladium(0); silver(I) nitrite; formic acid; sodium carbonate; toluene-4-sulfonic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
tetrahydrofuran; diethyl ether; ethanol; benzene;
DOI:10.1021/ol0613463
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 68 percent / AgNO2 / diethyl ether / 168 h / 20 °C
2: 81 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / 20 °C
3: 86 percent / p-toluenesulfonic acid / 20 °C
4: 84 percent / Na2CO3 / benzene / 24 h / 80 - 90 °C
5: 95 percent / formic acid; Pd(PPh3)4 / tetrahydrofuran / 24 h / Heating
6: ethanol / 1 h / 20 °C
With
tetrakis(triphenylphosphine) palladium(0); silver(I) nitrite; formic acid; sodium carbonate; toluene-4-sulfonic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
tetrahydrofuran; diethyl ether; ethanol; benzene;
DOI:10.1021/ol0613463
