S-benzyl-β-N-(furyl)methylenedithiocarbazate

Base Information

• Chemical Name: S-benzyl-β-N-(furyl)methylenedithiocarbazate
• CAS No.: 26155-84-0
• Molecular Formula: C₁₃H₁₂N₂OS₂
• Molecular Weight: 276.383
• Mol file: 26155-84-0.mol

Synonyms:S-benzyl-β-N-(furyl)methylenedithiocarbazate

Chemical Property of S-benzyl-β-N-(furyl)methylenedithiocarbazate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of S-benzyl-β-N-(furyl)methylenedithiocarbazate

There total 1 articles about S-benzyl-β-N-(furyl)methylenedithiocarbazate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

furfural (98-01-1) + S-benzyldithiocarbazate (13331-31-2) → S-benzyl-β-N-(furyl)methylenedithiocarbazate (26155-84-0)

Guidance literature:

In isopropyl alcohol; for 0.25h; Heating;

Reference yield: 78.0%

S-benzyl-β-N-(furyl)methylenedithiocarbazate (26155-84-0) + (2Z)-3-aza-2-bromo-1-(3-oxobenzo[f]chromen-2-yl)-3(phenylamino)prop-2-en-1-one (850832-70-1) → 2-(5-{[1-Furan-2-yl-meth-(E)-ylidene]-hydrazono}-4-phenyl-4,5-dihydro-[1,3,4]thiadiazole-2-carbonyl)-benzo[f]chromen-3-one

Guidance literature:

With triethylamine; In ethanol; for 30h;

DOI:10.1081/SCC-200048444

Reference yield:

S-benzyl-β-N-(furyl)methylenedithiocarbazate (26155-84-0) + C15H10BrN3OS → Benzothiazol-2-yl-(5-{[1-furan-2-yl-meth-(Z)-ylidene]-hydrazono}-4-phenyl-4,5-dihydro-[1,3,4]thiadiazol-2-yl)-methanone

Guidance literature:

With triethylamine; In ethanol; at 20 ℃; for 0.5h;

DOI:10.1080/10426500008082403

upstream raw materials:

furfural

S-benzyldithiocarbazate

Refernces

• 1、 Jadon, S. C. Singh,Gupta, Neeti,Singh, R. V.. "Synthetic and biochemical studies of some hydrazine carbodithioic acid derivatives of dioxomolybdenum (VI)". . p. 733 - 736. Retrieved 2007/10/03.
• 2、 Tarafder, M. T. H.,Rahim, M.. "Nickel complexes of S-benzyl-β-N-(furyl)methylenedithiocarbazate". . p. 1105 - 1107. Retrieved 2007/10/02.