C₂₀H₂₈O₇

Base Information

Chemical Name:C₂₀H₂₈O₇
CAS No.:1301166-57-3
Molecular Formula:C₂₀H₂₈O₇
Molecular Weight:380.438
Hs Code.:

C<sub>20</sub>H<sub>28</sub>O<sub>7</sub>

Synonyms:C₂₀H₂₈O₇

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Chemical Property of C₂₀H₂₈O₇

Chemical Property:

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Technology Process of C₂₀H₂₈O₇

There total 10 articles about C₂₀H₂₈O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1301166-63-1
C₁₇H₂₄O₆

: 88738-78-7
bis-(2,2,2-trifluoroethyl)(methoxycarbonylmethyl)phosphonate

: 1301166-57-3
C₂₀H₂₈O₇

Guidance literature:: With sodium hydride; In tetrahydrofuran;
DOI:10.1016/j.tetlet.2011.02.025

Reference yield:

: 1301166-51-7
C₁₀H₁₈O₅

: 1301166-57-3
C₂₀H₂₈O₇

Guidance literature:: Multi-step reaction with 6 steps

1.1: Nitrosobenzene; D-Prolin / dimethyl sulfoxide

1.2: 0.5 h

2.1: 1H-imidazole / dichloromethane / 1 h

3.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 2 h / 0 - 20 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C

5.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dichloromethane; dimethyl sulfoxide / 3 h / 20 °C

6.1: sodium hydride / tetrahydrofuran

With 1H-imidazole; tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; sodium hydride; Nitrosobenzene; D-Prolin; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; 1.1: MacMillan α-hydroxylation / 1.2: MacMillan α-hydroxylation / 1.3: MacMillan α-hydroxylation / 6.1: Still-Gennari cis-ofefination;
DOI:10.1016/j.tetlet.2011.02.025

Reference yield:

: C₁₁H₂₂O₆

: 1301166-57-3
C₂₀H₂₈O₇

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium periodate / 2 h / 20 °C

2.1: Nitrosobenzene; D-Prolin / dimethyl sulfoxide

2.2: 0.5 h

3.1: 1H-imidazole / dichloromethane / 1 h

4.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 2 h / 0 - 20 °C

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C

6.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dichloromethane; dimethyl sulfoxide / 3 h / 20 °C

7.1: sodium hydride / tetrahydrofuran

With 1H-imidazole; sodium periodate; tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; sodium hydride; Nitrosobenzene; D-Prolin; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; 2.1: MacMillan α-hydroxylation / 2.2: MacMillan α-hydroxylation / 2.3: MacMillan α-hydroxylation / 7.1: Still-Gennari cis-ofefination;
DOI:10.1016/j.tetlet.2011.02.025