C₃₀H₃₃NO₉

Base Information

Chemical Name:C₃₀H₃₃NO₉
CAS No.:910138-87-3
Molecular Formula:C₃₀H₃₃NO₉
Molecular Weight:551.593
Hs Code.:

C<sub>30</sub>H<sub>33</sub>NO<sub>9</sub>

Synonyms:C₃₀H₃₃NO₉

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Chemical Property of C₃₀H₃₃NO₉

Chemical Property:

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Technology Process of C₃₀H₃₃NO₉

There total 16 articles about C₃₀H₃₃NO₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: C₂₅H₂₅NO₇*ClH

: 910138-87-3
C₃₀H₃₃NO₉

Guidance literature:: With ytterbium(III) triflate; In dichloromethane; at 0 ℃; for 48h; Inert atmosphere;

Reference yield:

: 524939-61-5
1-[(4S,5S)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl]-1-[(tert-butyldimethylsilyloxy)methyl]-2-propen-1-ol

: 910138-87-3
C₃₀H₃₃NO₉

Guidance literature:: Multi-step reaction with 14 steps

1.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 24 h / 25 °C / Inert atmosphere

2.1: acetonitrile / 1 h / 0 °C / Inert atmosphere

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 5 h / 0 °C / Inert atmosphere

3.2: 0.5 h / 0 °C / Inert atmosphere

3.3: 0 - 25 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 25 °C / Inert atmosphere

5.1: sodium periodate / dichloromethane; water / 0.5 h / 25 °C / Inert atmosphere

6.1: triethylamine / tetrahydrofuran / 3 h / 25 °C / Inert atmosphere

7.1: caesium carbonate / 1,4-dioxane / 18 h / 25 - 100 °C / Inert atmosphere

8.1: caesium carbonate / tetrahydrofuran / 20 h / 25 °C / Inert atmosphere

9.1: silver trifluoromethanesulfonate / dichloromethane / 1 h / 25 °C / Inert atmosphere

9.2: -45 - 25 °C

10.1: tert-butyl alcohol / tetrahydrofuran / 0.17 h / 25 °C / Inert atmosphere

10.2: 0.17 h / -78 °C / Inert atmosphere

10.3: -78 - 25 °C / Inert atmosphere

11.1: Schwartz's reagent / tetrahydrofuran / 16 h / 25 - 40 °C / Inert atmosphere

12.1: potassium hexamethylsilazane / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

12.2: 1 h / 0 °C / Inert atmosphere

13.1: hydrogenchloride / methanol; water / 16 h / 25 °C / Inert atmosphere

14.1: ytterbium(III) triflate / dichloromethane / 48 h / 0 °C / Inert atmosphere

With hydrogenchloride; sodium periodate; Schwartz's reagent; tetrabutyl ammonium fluoride; silver trifluoromethanesulfonate; potassium hexamethylsilazane; caesium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; ytterbium(III) triflate; tert-butyl alcohol; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; acetonitrile;

Reference yield:

: 6-(2-benzo[1,3]dioxol-5-ylaziridin-1-yl).2,2.dimethyl-3a,6a-dihydrocyclopenta[1,3]dioxol-4-one

: 910138-87-3
C₃₀H₃₃NO₉

Guidance literature:: Multi-step reaction with 8 steps

1.1: caesium carbonate / 1,4-dioxane / 18 h / 25 - 100 °C / Inert atmosphere

2.1: caesium carbonate / tetrahydrofuran / 20 h / 25 °C / Inert atmosphere

3.1: silver trifluoromethanesulfonate / dichloromethane / 1 h / 25 °C / Inert atmosphere

3.2: -45 - 25 °C

4.1: tert-butyl alcohol / tetrahydrofuran / 0.17 h / 25 °C / Inert atmosphere

4.2: 0.17 h / -78 °C / Inert atmosphere

4.3: -78 - 25 °C / Inert atmosphere

5.1: Schwartz's reagent / tetrahydrofuran / 16 h / 25 - 40 °C / Inert atmosphere

6.1: potassium hexamethylsilazane / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

6.2: 1 h / 0 °C / Inert atmosphere

7.1: hydrogenchloride / methanol; water / 16 h / 25 °C / Inert atmosphere

8.1: ytterbium(III) triflate / dichloromethane / 48 h / 0 °C / Inert atmosphere

With hydrogenchloride; Schwartz's reagent; silver trifluoromethanesulfonate; potassium hexamethylsilazane; caesium carbonate; ytterbium(III) triflate; tert-butyl alcohol; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water;