C₂₃H₂₃N₅OS

Base Information

Chemical Name:C₂₃H₂₃N₅OS
CAS No.:1433962-18-5
Molecular Formula:C₂₃H₂₃N₅OS
Molecular Weight:417.535
Hs Code.:

C<sub>23</sub>H<sub>23</sub>N<sub>5</sub>OS

Synonyms:C₂₃H₂₃N₅OS

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Chemical Property of C₂₃H₂₃N₅OS

Chemical Property:

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Technology Process of C₂₃H₂₃N₅OS

There total 8 articles about C₂₃H₂₃N₅OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 178320-73-5
2,2-dimethyl-N-(prop-2-ynyl)propionamide

: 1433962-11-8
(E)-2-(4-azidostyryl)-1,3-benzothiazole

: 1433962-18-5
C₂₃H₂₃N₅OS

Guidance literature:: With bis(triphenylphosphino)copper(I) nitrate; triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1039/c3ob40296g

Reference yield:

: 120-75-2
2-Methylbenzothiazole

: 1433962-18-5
C₂₃H₂₃N₅OS

Guidance literature:: Multi-step reaction with 3 steps

1: sodium methylate / dimethyl sulfoxide / 20 h / 20 °C / Inert atmosphere

2: trifluoroacetic acid / toluene / 16 h / 60 - 70 °C / Molecular sieve

3: triethylamine; bis(triphenylphosphino)copper(I) nitrate / dichloromethane / 20 °C

With bis(triphenylphosphino)copper(I) nitrate; sodium methylate; triethylamine; trifluoroacetic acid; In dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1039/c3ob40296g

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 1433962-18-5
C₂₃H₂₃N₅OS

Guidance literature:: Multi-step reaction with 4 steps

1.1: p-toluenesulfonic acid monohydrate / toluene / 18 h / 110 °C / Sealed tube

2.1: tin(ll) chloride; hydrogenchloride / water / 20 °C

3.1: hydrogenchloride; sodium nitrite / water; methanol / 0 °C

3.2: 3 h / 0 - 20 °C

4.1: triethylamine; bis(triphenylphosphino)copper(I) nitrate / dichloromethane / 20 °C

With hydrogenchloride; bis(triphenylphosphino)copper(I) nitrate; p-toluenesulfonic acid monohydrate; triethylamine; tin(ll) chloride; sodium nitrite; In methanol; dichloromethane; water; toluene;
DOI:10.1039/c3ob40296g