(η⁵-1,2,3-tris[di-tert-butyl(methyl)silyl]-4-phenyl-1,2-disila-3-germacyclopentadienyl)(η5-pentamethylcyclopentadienyl)iron

Base Information

• Chemical Name: (η⁵-1,2,3-tris[di-tert-butyl(methyl)silyl]-4-phenyl-1,2-disila-3-germacyclopentadienyl)(η5-pentamethylcyclopentadienyl)iron
• CAS No.: 950783-81-0
• Molecular Formula: C₄₅H₈₄FeGeSi₅
• Molecular Weight: 894.026

Synonyms:(η⁵-1,2,3-tris[di-tert-butyl(methyl)silyl]-4-phenyl-1,2-disila-3-germacyclopentadienyl)(η5-pentamethylcyclopentadienyl)iron

Chemical Property of (η⁵-1,2,3-tris[di-tert-butyl(methyl)silyl]-4-phenyl-1,2-disila-3-germacyclopentadienyl)(η5-pentamethylcyclopentadienyl)iron

Chemical Property:

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Technology Process of (η⁵-1,2,3-tris[di-tert-butyl(methyl)silyl]-4-phenyl-1,2-disila-3-germacyclopentadienyl)(η5-pentamethylcyclopentadienyl)iron

There total 2 articles about (η⁵-1,2,3-tris[di-tert-butyl(methyl)silyl]-4-phenyl-1,2-disila-3-germacyclopentadienyl)(η5-pentamethylcyclopentadienyl)iron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

iron(II) acetylacetonate + C2GeSi2HC6H5(SiCH3(C(CH3)3)2)3(1-)*Li(1+)*C4H8O=C2HGeSi2C6H5(SiCH3(C(CH3)3)2)3Li*C4H8O + lithiumpentamethylcyclopentadiene → (η5-1,2,3-tris[di-tert-butyl(methyl)silyl]-4-phenyl-1,2-disila-3-germacyclopentadienyl)(η5-pentamethylcyclopentadienyl)iron (950783-81-0)

Guidance literature:

In tetrahydrofuran; Fe-complex reacted with Li-salts in THF at -78°C; silica gel chromy., recrystd. from pentane;

DOI:10.1021/ja0740162

Reference yield:

(η5-pentamethylcyclopentadienyl)Fe(acetylacetonate) (97210-26-9) + lithium disilagermacyclopentadienide (868164-37-8) → (η5-1,2,3-tris[di-tert-butyl(methyl)silyl]-4-phenyl-1,2-disila-3-germacyclopentadienyl)(η5-pentamethylcyclopentadienyl)iron (950783-81-0)

Guidance literature:

In tetrahydrofuran; at -78 - 20 ℃; for 0.75h; Sealed tube; Glovebox;

DOI:10.1246/bcsj.20130235

upstream raw materials:

(η5-pentamethylcyclopentadienyl)Fe(acetylacetonate)

lithium disilagermacyclopentadienide

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