1-(2'-aminophenyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-3-hydrazide

Base Information

Chemical Name:1-(2'-aminophenyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-3-hydrazide
CAS No.:86043-28-9
Molecular Formula:C₁₈H₁₉N₅O
Molecular Weight:321.382
Hs Code.:

Synonyms:1-(2'-aminophenyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-3-hydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2'-aminophenyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-3-hydrazide

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Technology Process of 1-(2'-aminophenyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-3-hydrazide

There total 4 articles about 1-(2'-aminophenyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-3-hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 86043-14-3
1-(2-Nitro-phenyl)-2,3,4,9-tetrahydro-1H-β-carboline-3-carboxylic acid hydrazide

: 86043-28-9
1-(2'-aminophenyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-3-hydrazide

Guidance literature:: With nickel; hydrazine hydrate; In ethanol; for 1h; Heating;

Reference yield:

: 497164-76-8
methyl-1-(2-nitrophenyl)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole-3-carboxylate

: 86043-28-9
1-(2'-aminophenyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-3-hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / hydrazine hydrate / ethanol / 4 h / Heating

2: 76 percent / hydrazine hydrate, Raney-Ni / ethanol / 1 h / Heating

With nickel; hydrazine hydrate; In ethanol;

Reference yield:

: 552-89-6
2-nitro-benzaldehyde

: 86043-28-9
1-(2'-aminophenyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-3-hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent

2: 86 percent / hydrazine hydrate / ethanol / 4 h / Heating

3: 76 percent / hydrazine hydrate, Raney-Ni / ethanol / 1 h / Heating

With nickel; hydrazine hydrate; In ethanol;