dibenzyl glycyl-L-aspartate trifluoroacetate

Base Information

Chemical Name:dibenzyl glycyl-L-aspartate trifluoroacetate
CAS No.:257940-90-2
Molecular Formula:C₂HF₃O₂*C₂₀H₂₂N₂O₅
Molecular Weight:484.429
Hs Code.:

Synonyms:dibenzyl glycyl-L-aspartate trifluoroacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dibenzyl glycyl-L-aspartate trifluoroacetate

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Technology Process of dibenzyl glycyl-L-aspartate trifluoroacetate

There total 3 articles about dibenzyl glycyl-L-aspartate trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 56612-93-2
dibenzyl N-(tert-butoxycarbonyl)glycyl-L-aspartate

: 257940-90-2
dibenzyl glycyl-L-aspartate trifluoroacetate

Guidance literature:: With trifluoroacetic acid; at 30 ℃; for 8h;
DOI:10.1016/j.ejmech.2019.111720

Reference yield: 90.0%

: 56612-93-2
dibenzyl N-(tert-butoxycarbonyl)glycyl-L-aspartate

: 76-05-1
trifluoroacetic acid

: 257940-90-2
dibenzyl glycyl-L-aspartate trifluoroacetate

Guidance literature:: In dichloromethane; at 20 ℃; for 24h;
DOI:10.1002/cbdv.201200261

Reference yield:

: 2791-79-9
dibenzyl L-aspartate

: 257940-90-2
dibenzyl glycyl-L-aspartate trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 4-methyl-morpholine; dicyclohexyl-carbodiimide; Succinimide / dichloromethane / 14 h / 20 °C / Inert atmosphere

2: dichloromethane / 24 h / 20 °C

With 4-methyl-morpholine; Succinimide; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1002/cbdv.201200261