Technology Process of Di-O-benzoyl-2-brom-2-deoxy-D-arabinosylbromid
There total 4 articles about Di-O-benzoyl-2-brom-2-deoxy-D-arabinosylbromid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine / dichloromethane / 2.78 h / -30 - -4 °C / Inert atmosphere
2: lithium bromide / 1-methyl-pyrrolidin-2-one / 20 h / 20 °C / Inert atmosphere
3: hydrogen bromide; acetic acid / dichloromethane / 23 h / 20 °C / Inert atmosphere
With
pyridine; hydrogen bromide; acetic acid; lithium bromide;
In
1-methyl-pyrrolidin-2-one; dichloromethane;
DOI:10.1021/op800182x
- Guidance literature:
-
With
hydrogen bromide; acetic acid;
In
dichloromethane;
at 20 ℃;
for 23h;
Inert atmosphere;
DOI:10.1021/op800182x
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium bromide / 1-methyl-pyrrolidin-2-one / 20 h / 20 °C / Inert atmosphere
2: hydrogen bromide; acetic acid / dichloromethane / 23 h / 20 °C / Inert atmosphere
With
hydrogen bromide; acetic acid; lithium bromide;
In
1-methyl-pyrrolidin-2-one; dichloromethane;
DOI:10.1021/op800182x
