Di-O-benzoyl-2-brom-2-deoxy-D-arabinosylbromid

Base Information

Chemical Name:Di-O-benzoyl-2-brom-2-deoxy-D-arabinosylbromid
CAS No.:55734-52-6
Molecular Formula:C₁₉H₁₆Br₂O₅
Molecular Weight:484.141
Hs Code.:

Synonyms:Di-O-benzoyl-2-brom-2-deoxy-D-arabinosylbromid

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Chemical Property of Di-O-benzoyl-2-brom-2-deoxy-D-arabinosylbromid

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Technology Process of Di-O-benzoyl-2-brom-2-deoxy-D-arabinosylbromid

There total 4 articles about Di-O-benzoyl-2-brom-2-deoxy-D-arabinosylbromid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22224-41-5
1,3,5-tri-O-benzoyl-α-D-ribofuranoside

: 55734-52-6
Di-O-benzoyl-2-brom-2-deoxy-D-arabinosylbromid

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / dichloromethane / 2.78 h / -30 - -4 °C / Inert atmosphere

2: lithium bromide / 1-methyl-pyrrolidin-2-one / 20 h / 20 °C / Inert atmosphere

3: hydrogen bromide; acetic acid / dichloromethane / 23 h / 20 °C / Inert atmosphere

With pyridine; hydrogen bromide; acetic acid; lithium bromide; In 1-methyl-pyrrolidin-2-one; dichloromethane;
DOI:10.1021/op800182x

Reference yield:

: C₂₆H₂₁BrO₇

: 55734-52-6
Di-O-benzoyl-2-brom-2-deoxy-D-arabinosylbromid

Guidance literature:: With hydrogen bromide; acetic acid; In dichloromethane; at 20 ℃; for 23h; Inert atmosphere;
DOI:10.1021/op800182x

Reference yield:

: 97614-41-0
2-O-<(trifluoromethyl)sulfonyl>-1,3,5-tri-O-benzoyl-α-D-ribofuranose

: 55734-52-6
Di-O-benzoyl-2-brom-2-deoxy-D-arabinosylbromid

Guidance literature:: Multi-step reaction with 2 steps

1: lithium bromide / 1-methyl-pyrrolidin-2-one / 20 h / 20 °C / Inert atmosphere

2: hydrogen bromide; acetic acid / dichloromethane / 23 h / 20 °C / Inert atmosphere

With hydrogen bromide; acetic acid; lithium bromide; In 1-methyl-pyrrolidin-2-one; dichloromethane;
DOI:10.1021/op800182x