[1,2-bis(diphenylphosphino)ethane]chloro(phenylazoacetaldoximato)palladium(II)

Base Information

Chemical Name:[1,2-bis(diphenylphosphino)ethane]chloro(phenylazoacetaldoximato)palladium(II)
CAS No.:75662-87-2
Molecular Formula:C₃₄H₃₂ClN₃OP₂Pd
Molecular Weight:702.468
Hs Code.:

Synonyms:[1,2-bis(diphenylphosphino)ethane]chloro(phenylazoacetaldoximato)palladium(II)

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Chemical Property of [1,2-bis(diphenylphosphino)ethane]chloro(phenylazoacetaldoximato)palladium(II)

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Technology Process of [1,2-bis(diphenylphosphino)ethane]chloro(phenylazoacetaldoximato)palladium(II)

There total 2 articles about [1,2-bis(diphenylphosphino)ethane]chloro(phenylazoacetaldoximato)palladium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: di-μ-chlorobis[α-phenylazoacetaldoximato-N,N''palladium(II)]

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: 75662-87-2
[1,2-bis(diphenylphosphino)ethane]chloro(phenylazoacetaldoximato)palladium(II)

Guidance literature:: In benzene; stirring at 298 K for 15 min; crystals filtered off, washed with benzene, dried in vac.; elem. anal.;
DOI:10.1039/DT9800001698

Reference yield:

: phenyldiazenylacetaldoxime

: 75662-87-2
[1,2-bis(diphenylphosphino)ethane]chloro(phenylazoacetaldoximato)palladium(II)

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol

2: benzene

In ethanol; benzene;
DOI:10.1039/DT9800001698

Reference yield:

: 75662-87-2
[1,2-bis(diphenylphosphino)ethane]chloro(phenylazoacetaldoximato)palladium(II)

: 19978-61-1
(1,2-bis(diphenylphosphanyl)ethane)dichloridopalladium(II)

Guidance literature:: With HCl; In chloroform; byproducts: phenylazoacetaldoxime; passage of HCl gas continued until colour of soln. turned to yellow at 298 K; Pd-complex crystd. out, phenylazoacetaldoxime obtained by evapg. the filtrate;
DOI:10.1039/DT9800001698