(4S,5S,αR)-4-tert-butoxycarbonyl-5-(N-benzyl-N-α-methylbenzylamino)-5-phenyl-pentanoic acid

Base Information

Chemical Name:(4S,5S,αR)-4-tert-butoxycarbonyl-5-(N-benzyl-N-α-methylbenzylamino)-5-phenyl-pentanoic acid
CAS No.:1026773-48-7
Molecular Formula:C₃₁H₃₇NO₄
Molecular Weight:487.639
Hs Code.:

Synonyms:(4S,5S,αR)-4-tert-butoxycarbonyl-5-(N-benzyl-N-α-methylbenzylamino)-5-phenyl-pentanoic acid

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Chemical Property of (4S,5S,αR)-4-tert-butoxycarbonyl-5-(N-benzyl-N-α-methylbenzylamino)-5-phenyl-pentanoic acid

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Technology Process of (4S,5S,αR)-4-tert-butoxycarbonyl-5-(N-benzyl-N-α-methylbenzylamino)-5-phenyl-pentanoic acid

There total 2 articles about (4S,5S,αR)-4-tert-butoxycarbonyl-5-(N-benzyl-N-α-methylbenzylamino)-5-phenyl-pentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1026773-43-2
C₁₆H₂₀O₄

: 38235-77-7
(R)-N-benzyl-1-phenylethylamine

: C₂₉H₃₃NO₂

: 1026773-48-7
(4S,5S,αR)-4-tert-butoxycarbonyl-5-(N-benzyl-N-α-methylbenzylamino)-5-phenyl-pentanoic acid

: C₄₄H₅₀N₂O₂

: 1026773-59-0
C₄₄H₅₀N₂O₂

Guidance literature:: (R)-N-benzyl-1-phenylethylamine; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

C₁₆H₂₀O₄; In tetrahydrofuran; at -78 ℃; Inert atmosphere;

With water; ammonium chloride; In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1021/ol8001464

Reference yield: 51.0%

: 38235-77-7
(R)-N-benzyl-1-phenylethylamine

: 159999-60-7
tert-butyl 3-acetoxy-2-methylene-3-phenylpropanoate

: 1026773-48-7
(4S,5S,αR)-4-tert-butoxycarbonyl-5-(N-benzyl-N-α-methylbenzylamino)-5-phenyl-pentanoic acid

: 1026773-59-0
C₄₄H₅₀N₂O₂

Guidance literature:: (R)-N-benzyl-1-phenylethylamine; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

tert-butyl 3-acetoxy-2-methylene-3-phenylpropanoate; In tetrahydrofuran; at -78 ℃; Inert atmosphere;

With water; ammonium chloride; In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1021/ol8001464