Technology Process of N1-p-acetamidobenzyl-N3-n-propyl-5,6-diaminouracil
There total 6 articles about N1-p-acetamidobenzyl-N3-n-propyl-5,6-diaminouracil which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
nickel;
In
ethanol;
for 4h;
under 760 Torr;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 74 percent / Ac2O / 20 h / 50 °C
2: 92 percent / conc NaOH / ethanol / 1 h
3: H2 / PtO2 / ethanol / 3 h / 760 Torr / Ambient temperature
4: 91 percent / pyridine / 2 h / 0 °C
5: 89 percent / NaNO2 / methanol; acetic acid; H2O / 3 h / Ambient temperature
6: H2 / Raney Ni / ethanol / 4 h / 760 Torr / Ambient temperature
With
sodium hydroxide; hydrogen; acetic anhydride; sodium nitrite;
platinum(IV) oxide; nickel;
In
pyridine; methanol; ethanol; water; acetic acid;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 92 percent / conc NaOH / ethanol / 1 h
2: H2 / PtO2 / ethanol / 3 h / 760 Torr / Ambient temperature
3: 91 percent / pyridine / 2 h / 0 °C
4: 89 percent / NaNO2 / methanol; acetic acid; H2O / 3 h / Ambient temperature
5: H2 / Raney Ni / ethanol / 4 h / 760 Torr / Ambient temperature
With
sodium hydroxide; hydrogen; sodium nitrite;
platinum(IV) oxide; nickel;
In
pyridine; methanol; ethanol; water; acetic acid;
