N-{5-[2-(N,N-dimethylsulfamoyl)-4,5-dimethoxybenzyl]-1,3,4-thiadiazol-2-yl}-N-butylamine

Base Information

Chemical Name:N-{5-[2-(N,N-dimethylsulfamoyl)-4,5-dimethoxybenzyl]-1,3,4-thiadiazol-2-yl}-N-butylamine
CAS No.:1360593-75-4
Molecular Formula:C₁₇H₂₆N₄O₄S₂
Molecular Weight:414.55
Hs Code.:

Synonyms:N-{5-[2-(N,N-dimethylsulfamoyl)-4,5-dimethoxybenzyl]-1,3,4-thiadiazol-2-yl}-N-butylamine

Suppliers and Price of N-{5-[2-(N,N-dimethylsulfamoyl)-4,5-dimethoxybenzyl]-1,3,4-thiadiazol-2-yl}-N-butylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-{5-[2-(N,N-dimethylsulfamoyl)-4,5-dimethoxybenzyl]-1,3,4-thiadiazol-2-yl}-N-butylamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-{5-[2-(N,N-dimethylsulfamoyl)-4,5-dimethoxybenzyl]-1,3,4-thiadiazol-2-yl}-N-butylamine

There total 3 articles about N-{5-[2-(N,N-dimethylsulfamoyl)-4,5-dimethoxybenzyl]-1,3,4-thiadiazol-2-yl}-N-butylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1360593-53-8
1-[((N,N-dimethylsulfamoyl)-4,5-dimethoxyphenyl)acetyl]-4-butylthiosemicarbazide

: 1360593-75-4
N-{5-[2-(N,N-dimethylsulfamoyl)-4,5-dimethoxybenzyl]-1,3,4-thiadiazol-2-yl}-N-butylamine

Guidance literature:: 1-[((N,N-dimethylsulfamoyl)-4,5-dimethoxyphenyl)acetyl]-4-butylthiosemicarbazide; With sulfuric acid; at 20 ℃; for 0.75h; Cooling;

With ammonia; In water; pH=8; Cooling with ice;
DOI:10.1016/j.bmc.2011.12.031

Reference yield:

: 1016637-96-9
2-(2-hydrazinyl-2-oxoethyl)-N,N-dimethyl-4,5-dimethoxybenzenesulfonamide

: 1360593-75-4
N-{5-[2-(N,N-dimethylsulfamoyl)-4,5-dimethoxybenzyl]-1,3,4-thiadiazol-2-yl}-N-butylamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: ethanol / 1 h / Reflux

2.1: sulfuric acid / 0.75 h / 20 °C / Cooling

2.2: pH 8 / Cooling with ice

With sulfuric acid; In ethanol;
DOI:10.1016/j.bmc.2011.12.031

Reference yield:

: 592-82-5
butyl isothiocyanate

: 1360593-75-4
N-{5-[2-(N,N-dimethylsulfamoyl)-4,5-dimethoxybenzyl]-1,3,4-thiadiazol-2-yl}-N-butylamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: ethanol / 1 h / Reflux

2.1: sulfuric acid / 0.75 h / 20 °C / Cooling

2.2: pH 8 / Cooling with ice

With sulfuric acid; In ethanol;
DOI:10.1016/j.bmc.2011.12.031