Technology Process of C24H24N4O2
There total 5 articles about C24H24N4O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C20H20ClN3O2; 1-(triisopropylsilyl)-1H-pyrrole-3-boronic acid;
With
tetrakis(triphenylphosphine) palladium(0); sodium carbonate;
In
1,2-dimethoxyethane; water;
at 100 ℃;
for 4h;
Inert atmosphere;
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran; 1,2-dimethoxyethane; water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium t-butanolate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium diacetate / 1,2-dimethoxyethane / 5 h / Inert atmosphere; Reflux
2.1: trichlorophosphate / 0.67 h / 80 °C
3.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 5 °C / Inert atmosphere
3.2: 1.83 h / 5 - 20 °C
4.1: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 4 h / 100 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); palladium diacetate; sodium hydride; sodium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; trichlorophosphate;
In
1,2-dimethoxyethane; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium t-butanolate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium diacetate / 1,2-dimethoxyethane / 5 h / Inert atmosphere; Reflux
2.1: trichlorophosphate / 0.67 h / 80 °C
3.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 5 °C / Inert atmosphere
3.2: 1.83 h / 5 - 20 °C
4.1: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 4 h / 100 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); palladium diacetate; sodium hydride; sodium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; trichlorophosphate;
In
1,2-dimethoxyethane; water; N,N-dimethyl-formamide;