3-(3,4-dimethoxyphenyl)-2-(2-hydroxymethyl-4,5-dimethoxyphenyl)propionohydrazide

Base Information

Chemical Name:3-(3,4-dimethoxyphenyl)-2-(2-hydroxymethyl-4,5-dimethoxyphenyl)propionohydrazide
CAS No.:76056-02-5
Molecular Formula:C₂₀H₂₆N₂O₆
Molecular Weight:390.436
Hs Code.:

Synonyms:3-(3,4-dimethoxyphenyl)-2-(2-hydroxymethyl-4,5-dimethoxyphenyl)propionohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(3,4-dimethoxyphenyl)-2-(2-hydroxymethyl-4,5-dimethoxyphenyl)propionohydrazide

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Technology Process of 3-(3,4-dimethoxyphenyl)-2-(2-hydroxymethyl-4,5-dimethoxyphenyl)propionohydrazide

There total 2 articles about 3-(3,4-dimethoxyphenyl)-2-(2-hydroxymethyl-4,5-dimethoxyphenyl)propionohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 76055-91-9
4-(3,4-dimethoxybenzyl)-6,7-dimethoxyisochroman-3-one

: 76056-02-5
3-(3,4-dimethoxyphenyl)-2-(2-hydroxymethyl-4,5-dimethoxyphenyl)propionohydrazide

Guidance literature:: With hydrazine hydrate; In ethanol; for 6h; Heating;

Reference yield:

: 76055-90-8
2-(2-hydroxymethyl-4,5-dimethoxyphenyl)-3-(3,4-dimethoxyphenyl)-N-methylpropionamide

: 76056-02-5
3-(3,4-dimethoxyphenyl)-2-(2-hydroxymethyl-4,5-dimethoxyphenyl)propionohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / toluene-4-sulphonyl chloride / pyridine / 5 h / Heating

2: 82 percent / hydrazine hydrate / ethanol / 6 h / Heating

With hydrazine hydrate; p-toluenesulfonyl chloride; In pyridine; ethanol;