Technology Process of C45H62OS2
There total 3 articles about C45H62OS2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
tetrahydrofuran; methanol;
at 20 ℃;
for 8h;
DOI:10.1002/chem.201102260
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1 h / Reflux
2: potassium tert-butylate / tetrahydrofuran / 2 h / 0 - 20 °C
3: trichlorophosphate / 1,1-Dichloroethylene / Reflux
4: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine / 20 °C
5: potassium carbonate / tetrahydrofuran; methanol / 8 h / 20 °C
With
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); potassium tert-butylate; potassium carbonate; triethylamine; trichlorophosphate;
In
tetrahydrofuran; methanol; 1,1-Dichloroethylene;
3: Vilsmeier formylation / 4: Sonogashira coupling;
DOI:10.1002/chem.201102260
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium tert-butylate / tetrahydrofuran / 2 h / 0 - 20 °C
2: trichlorophosphate / 1,1-Dichloroethylene / Reflux
3: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine / 20 °C
4: potassium carbonate / tetrahydrofuran; methanol / 8 h / 20 °C
With
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); potassium tert-butylate; potassium carbonate; triethylamine; trichlorophosphate;
In
tetrahydrofuran; methanol; 1,1-Dichloroethylene;
2: Vilsmeier formylation / 3: Sonogashira coupling;
DOI:10.1002/chem.201102260
