1H-[1,3]Diazepino[1,2-a]benzimidazole,2,3,4,5-tetrahydro-(9CI)

Base Information

Chemical Name:1H-[1,3]Diazepino[1,2-a]benzimidazole,2,3,4,5-tetrahydro-(9CI)
CAS No.:143262-60-6
Molecular Formula:C11H13 N3
Molecular Weight:187.244
Hs Code.:
Mol file:143262-60-6.mol

Synonyms:1H-[1,3]Diazepino[1,2-a]benzimidazole,2,3,4,5-tetrahydro- (9CI)

Suppliers and Price of 1H-[1,3]Diazepino[1,2-a]benzimidazole,2,3,4,5-tetrahydro-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AccelPharmtech
2,4,5,11-tetrahydro-3H-[1,3]Diazepino[1,2-a]benzimidazole 97.00%
5G
$ 6050.00

AccelPharmtech
2,4,5,11-tetrahydro-3H-[1,3]Diazepino[1,2-a]benzimidazole 97.00%
1G
$ 3510.00

Total 1 raw suppliers

Chemical Property of 1H-[1,3]Diazepino[1,2-a]benzimidazole,2,3,4,5-tetrahydro-(9CI)

Chemical Property:

PSA：29.85000
LogP:2.38000

Purity/Quality:: 2,4,5,11-tetrahydro-3H-[1,3]Diazepino[1,2-a]benzimidazole 97.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1H-[1,3]Diazepino[1,2-a]benzimidazole,2,3,4,5-tetrahydro-(9CI)

There total 5 articles about 1H-[1,3]Diazepino[1,2-a]benzimidazole,2,3,4,5-tetrahydro-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1-acetyl-2,3,4,5-tetrahydro[1,3]diazepino[1,2-a]benzimidazole

: 143262-60-6
1⁽¹¹⁾H-2,3,4,5-tetrahydro[1,3]diazepino[1,2-a]benzimidazole

Guidance literature:: With hydrogenchloride; for 1h; Heating;
DOI:10.1007/s11172-007-0366-8

Reference yield: 88.0%

: 143262-49-1
2-Phenyl-tetrahydro-pyridazine-1-carbonitrile

: 143262-60-6
1⁽¹¹⁾H-2,3,4,5-tetrahydro[1,3]diazepino[1,2-a]benzimidazole

Guidance literature:: In 1,2-dichloro-benzene; for 120h; Heating;
DOI:10.1016/S0040-4020(01)89022-0

Reference yield:

: 64661-86-5
benzenediazocyanide

: 143262-60-6
1⁽¹¹⁾H-2,3,4,5-tetrahydro[1,3]diazepino[1,2-a]benzimidazole

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / CH₂Cl₂

2: 78 percent / H₂ / PtO₂ / methanol / 48 h / 1810.02 Torr

3: 88 percent / 1,2-dichloro-benzene / 120 h / Heating

With hydrogen; platinum(IV) oxide; In methanol; dichloromethane; 1,2-dichloro-benzene;
DOI:10.1016/S0040-4020(01)89022-0