C₁₀₂H₁₃₂N₄O₁₂S₃

Base Information

• Chemical Name: C₁₀₂H₁₃₂N₄O₁₂S₃
• CAS No.: 1372853-30-9
• Molecular Formula: C₁₀₂H₁₃₂N₄O₁₂S₃
• Molecular Weight: 1702.39
• Mol file: 1372853-30-9.mol

Synonyms:C₁₀₂H₁₃₂N₄O₁₂S₃

Chemical Property of C₁₀₂H₁₃₂N₄O₁₂S₃

Chemical Property:

Purity/Quality:

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Technology Process of C₁₀₂H₁₃₂N₄O₁₂S₃

There total 1 articles about C₁₀₂H₁₃₂N₄O₁₂S₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

tris[2-(N-tosylaminoethyl)]amine (98846-92-5) + 5,11,17,23,29,35-hexa-tert-butyl-37,39,41-trimethoxy-38,40,42-tris(2-tosyloxyethoxy)calix[6]arene (529019-17-8) → C102H132N4O12S3 (1372853-30-9)

Guidance literature:

With potassium carbonate; caesium carbonate; In N,N-dimethyl-formamide; at 20 - 90 ℃; Inert atmosphere;

DOI:10.1021/jo300179h

Reference yield: 93.0%

C102H132N4O12S3 (1372853-30-9) → C90H105N7O18S3

Guidance literature:

With nitric acid; acetic acid; In dichloromethane; at 0 - 20 ℃; regioselective reaction; Inert atmosphere;

DOI:10.1021/jo300179h

upstream raw materials:

tris[2-(N-tosylaminoethyl)]amine

5,11,17,23,29,35-hexa-tert-butyl-37,39,41-trimethoxy-38,40,42-tris(2-tosyloxyethoxy)calix[6]arene