C₃₀H₅₂O₆Si

Base Information

Chemical Name:C₃₀H₅₂O₆Si
CAS No.:1300040-19-0
Molecular Formula:C₃₀H₅₂O₆Si
Molecular Weight:536.825
Hs Code.:

C<sub>30</sub>H<sub>52</sub>O<sub>6</sub>Si

Synonyms:C₃₀H₅₂O₆Si

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Chemical Property of C₃₀H₅₂O₆Si

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Technology Process of C₃₀H₅₂O₆Si

There total 8 articles about C₃₀H₅₂O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₈H₄₈O₅Si

: 107-30-2
chloromethyl methyl ether

: 1300040-19-0
C₃₀H₅₂O₆Si

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2011.02.061

Reference yield:

: 1300040-10-1
C₂₃H₃₂O₅

: 1300040-19-0
C₃₀H₅₂O₆Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydroxide / tetrahydrofuran; water / 40 °C

1.2: 20 °C

2.1: triethyl borane; oxygen; tri-n-butyl-tin hydride / toluene / -30 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

4.1: dmap; triethylamine / dichloromethane / -10 °C / Inert atmosphere

5.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 20 °C

6.1: sodium tetrahydroborate / methanol / -10 °C

7.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

With dmap; sodium tetrahydroborate; lithium aluminium tetrahydride; triethyl borane; oxygen; tri-n-butyl-tin hydride; sodium hydrogencarbonate; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; toluene;
DOI:10.1016/j.tet.2011.02.061

Reference yield:

: C₂₂H₃₄O₅

: 1300040-19-0
C₃₀H₅₂O₆Si

Guidance literature:: Multi-step reaction with 4 steps

1: dmap; triethylamine / dichloromethane / -10 °C / Inert atmosphere

2: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 20 °C

3: sodium tetrahydroborate / methanol / -10 °C

4: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

With dmap; sodium tetrahydroborate; sodium hydrogencarbonate; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane;
DOI:10.1016/j.tet.2011.02.061