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Technology Process of Hf(C5(CH3)5)2(CH2CH(CH3)2)(P(CH3)3)(1+)*B(C6H5)4(1-)=(Hf(C5(CH3)5)2(CH2CH(CH3)2)(P(CH3)3))(B(C6H5)4)

Hf(C5(CH3)5)2(CH2CH(CH3)2)(P(CH3)3)(1+)*B(C6H5)4(1-)=(Hf(C5(CH3)5)2(CH2CH(CH3)2)(P(CH3)3))(B(C6H5)4)

Base Information
  • Chemical Name:Hf(C5(CH3)5)2(CH2CH(CH3)2)(P(CH3)3)(1+)*B(C6H5)4(1-)=(Hf(C5(CH3)5)2(CH2CH(CH3)2)(P(CH3)3))(B(C6H5)4)
  • CAS No.:156278-75-0
  • Molecular Formula:C24H20B*C27H48HfP
  • Molecular Weight:901.376
  • Hs Code.:
Hf(C<sub>5</sub>(CH<sub>3</sub>)5)2(CH<sub>2</sub>CH(CH<sub>3</sub>)2)(P(CH<sub>3</sub>)3)<sup>(1+)</sup>*B(C<sub>6</sub>H<sub>5</sub>)4<sup>(1-)</sup>=(Hf(C<sub>5</sub>(CH<sub>3</sub>)5)2(CH<sub>2</sub>CH(CH<sub>3</sub>)2)(P(CH<sub>3</sub>)3))(B(C<sub>6</sub>H<sub>5</sub>)4)

Synonyms:Hf(C5(CH3)5)2(CH2CH(CH3)2)(P(CH3)3)(1+)*B(C6H5)4(1-)=(Hf(C5(CH3)5)2(CH2CH(CH3)2)(P(CH3)3))(B(C6H5)4)

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Chemical Property of Hf(C5(CH3)5)2(CH2CH(CH3)2)(P(CH3)3)(1+)*B(C6H5)4(1-)=(Hf(C5(CH3)5)2(CH2CH(CH3)2)(P(CH3)3))(B(C6H5)4)
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Technology Process of Hf(C5(CH3)5)2(CH2CH(CH3)2)(P(CH3)3)(1+)*B(C6H5)4(1-)=(Hf(C5(CH3)5)2(CH2CH(CH3)2)(P(CH3)3))(B(C6H5)4)

There total 1 articles about Hf(C5(CH3)5)2(CH2CH(CH3)2)(P(CH3)3)(1+)*B(C6H5)4(1-)=(Hf(C5(CH3)5)2(CH2CH(CH3)2)(P(CH3)3))(B(C6H5)4) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

Hf(C<sub>5</sub>(CH<sub>3</sub>)5)2(CH<sub>2</sub>CH(CH<sub>3</sub>)CH<sub>2</sub>)
105931-10-0

Hf(C5(CH3)5)2(CH2CH(CH3)CH2)

tri(n-butyl)ammonium tetraphenylborate
64167-39-1

tri(n-butyl)ammonium tetraphenylborate

Hf(C<sub>5</sub>(CH<sub>3</sub>)5)2(CH<sub>2</sub>CH(CH<sub>3</sub>)2)(P(CH<sub>3</sub>)3)<sup>(1+)</sup>*B(C<sub>6</sub>H<sub>5</sub>)4<sup>(1-)</sup>=(Hf(C<sub>5</sub>(CH<sub>3</sub>)5)2(CH<sub>2</sub>CH(CH<sub>3</sub>)2)(P(CH<sub>3</sub>)3))(B(C<sub>6</sub>H<sub>5</sub>)4)
156278-75-0

Hf(C5(CH3)5)2(CH2CH(CH3)2)(P(CH3)3)(1+)*B(C6H5)4(1-)=(Hf(C5(CH3)5)2(CH2CH(CH3)2)(P(CH3)3))(B(C6H5)4)

Guidance literature:
With PMe3; In dichloromethane-d2; to Hf-compd. and (HNBu3)BPH4 CD2Cl2 and PMe3 are added by vacuum transfer at -196°C (N2); tube is warmed to -78°C, agitated and allowed to warm to -10°C (15 min), tube is maintained at -78°C prior to NMR;
upstream raw materials:

Hf(C5(CH3)5)2(CH2CH(CH3)CH2)

tri(n-butyl)ammonium tetraphenylborate

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