ethanesulfonic acid [3-(6-chloro-4,4-dimethyl-1,2,3,4-tetrahydro-quinolin-2-yl)-phenyl]-amide

Base Information

Chemical Name:ethanesulfonic acid [3-(6-chloro-4,4-dimethyl-1,2,3,4-tetrahydro-quinolin-2-yl)-phenyl]-amide
CAS No.:1373546-14-5
Molecular Formula:C₁₉H₂₃ClN₂O₂S
Molecular Weight:378.923
Hs Code.:

Synonyms:ethanesulfonic acid [3-(6-chloro-4,4-dimethyl-1,2,3,4-tetrahydro-quinolin-2-yl)-phenyl]-amide

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Chemical Property of ethanesulfonic acid [3-(6-chloro-4,4-dimethyl-1,2,3,4-tetrahydro-quinolin-2-yl)-phenyl]-amide

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Technology Process of ethanesulfonic acid [3-(6-chloro-4,4-dimethyl-1,2,3,4-tetrahydro-quinolin-2-yl)-phenyl]-amide

There total 5 articles about ethanesulfonic acid [3-(6-chloro-4,4-dimethyl-1,2,3,4-tetrahydro-quinolin-2-yl)-phenyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1373547-09-1
3-(6-chloro-4,4-dimethyl-1,2,3,4-tetrahydro-quinolin-2-yl)-phenylamine

: 594-44-5
Ethanesulfonyl chloride

: 1373546-14-5
ethanesulfonic acid [3-(6-chloro-4,4-dimethyl-1,2,3,4-tetrahydro-quinolin-2-yl)-phenyl]-amide

Guidance literature:: With pyridine; at 20 ℃;

Reference yield:

: 99-61-6
3-nitro-benzaldehyde

: 1373546-14-5
ethanesulfonic acid [3-(6-chloro-4,4-dimethyl-1,2,3,4-tetrahydro-quinolin-2-yl)-phenyl]-amide

Guidance literature:: Multi-step reaction with 4 steps

1: toluene / 3 h / dean-stark trap; Reflux

2: boron trifluoride diethyl etherate / acetonitrile / 72 h / 20 °C / autoclave

3: water; iron / ethanol / 2 h / Reflux

4: pyridine / 20 °C

With pyridine; water; iron; boron trifluoride diethyl etherate; In ethanol; toluene; acetonitrile;

Reference yield:

: 106-47-8
4-chloro-aniline

: 1373546-14-5
ethanesulfonic acid [3-(6-chloro-4,4-dimethyl-1,2,3,4-tetrahydro-quinolin-2-yl)-phenyl]-amide

Guidance literature:: Multi-step reaction with 4 steps

1: toluene / 3 h / dean-stark trap; Reflux

2: boron trifluoride diethyl etherate / acetonitrile / 72 h / 20 °C / autoclave

3: water; iron / ethanol / 2 h / Reflux

4: pyridine / 20 °C

With pyridine; water; iron; boron trifluoride diethyl etherate; In ethanol; toluene; acetonitrile;