4-methyl-3-[[4-(3-pyridinyl)-2-pyrimidinyl]amino]benzenesulfonic acid N'-(2,4,6-trichlorobenzoyl)hydrazide

Base Information

Chemical Name:4-methyl-3-[[4-(3-pyridinyl)-2-pyrimidinyl]amino]benzenesulfonic acid N'-(2,4,6-trichlorobenzoyl)hydrazide
CAS No.:1186620-29-0
Molecular Formula:C₂₃H₁₇Cl₃N₆O₃S
Molecular Weight:563.851
Hs Code.:

Synonyms:4-methyl-3-[[4-(3-pyridinyl)-2-pyrimidinyl]amino]benzenesulfonic acid N'-(2,4,6-trichlorobenzoyl)hydrazide

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Chemical Property of 4-methyl-3-[[4-(3-pyridinyl)-2-pyrimidinyl]amino]benzenesulfonic acid N'-(2,4,6-trichlorobenzoyl)hydrazide

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Technology Process of 4-methyl-3-[[4-(3-pyridinyl)-2-pyrimidinyl]amino]benzenesulfonic acid N'-(2,4,6-trichlorobenzoyl)hydrazide

There total 3 articles about 4-methyl-3-[[4-(3-pyridinyl)-2-pyrimidinyl]amino]benzenesulfonic acid N'-(2,4,6-trichlorobenzoyl)hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1186620-62-1
4-methyl-3-[[4-(3-pyridinyl)-2-pyrimidinyl]amino]benzenesulfonyl chloride

: 2,4,6-trichlorobenzoylhydrazine

: 1186620-29-0
4-methyl-3-[[4-(3-pyridinyl)-2-pyrimidinyl]amino]benzenesulfonic acid N'-(2,4,6-trichlorobenzoyl)hydrazide

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 70 ℃; for 3h;

Reference yield:

: 37557-40-7
N-(2-methylphenyl)guanidine

: 1186620-29-0
4-methyl-3-[[4-(3-pyridinyl)-2-pyrimidinyl]amino]benzenesulfonic acid N'-(2,4,6-trichlorobenzoyl)hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / ISOPROPYLAMIDE / 12 h / 111 °C

2: chlorosulfonic acid / 0 °C

3: triethylamine / N,N-dimethyl-formamide / 3 h / 70 °C

With chlorosulfonic acid; potassium carbonate; triethylamine; In ISOPROPYLAMIDE; N,N-dimethyl-formamide;

Reference yield:

: 55314-16-4,75415-01-9,123367-26-0
3-(N,N-dimethylamino)-1-(pyridin-3-yl)prop-2-en-1-one

: 1186620-29-0
4-methyl-3-[[4-(3-pyridinyl)-2-pyrimidinyl]amino]benzenesulfonic acid N'-(2,4,6-trichlorobenzoyl)hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / ISOPROPYLAMIDE / 12 h / 111 °C

2: chlorosulfonic acid / 0 °C

3: triethylamine / N,N-dimethyl-formamide / 3 h / 70 °C

With chlorosulfonic acid; potassium carbonate; triethylamine; In ISOPROPYLAMIDE; N,N-dimethyl-formamide;