2(S)--3-phenylpropanimino ethyl ether

Base Information

Chemical Name:2(S)--3-phenylpropanimino ethyl ether
CAS No.:132402-59-6
Molecular Formula:C₁₆H₂₄N₂O₃
Molecular Weight:292.378
Hs Code.:

2(S)-<N-(tert-butyloxycarbonyl)amino>-3-phenylpropanimino ethyl ether

Synonyms:2(S)--3-phenylpropanimino ethyl ether

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Chemical Property of 2(S)--3-phenylpropanimino ethyl ether

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Technology Process of 2(S)--3-phenylpropanimino ethyl ether

There total 4 articles about 2(S)--3-phenylpropanimino ethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 88463-18-7,35150-06-2
(S)-2-[(tert-butoxycarbonyl)amino]-3-phenylpropionamide

: 17950-40-2
triethyloxonium hexaflourophosphate

: 132402-59-6
2(S)--3-phenylpropanimino ethyl ether

Guidance literature:: In dichloromethane; Ambient temperature;
DOI:10.1016/S0040-4020(01)81482-4

Reference yield:

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 132402-59-6
2(S)--3-phenylpropanimino ethyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) N-methylmorpholine, isobutyl chloroformate, 2.) NH₃ / 1) CH₂Cl₂, , -20 deg C, 30 min; 2) CH₂Cl₂, -20 deg C, 15 min, -20 deg C --> rt, 1 h

2: 98 percent / CH₂Cl₂ / 18 h / Ambient temperature

With 4-methyl-morpholine; ammonia; isobutyl chloroformate; In dichloromethane;
DOI:10.1021/jo9613491

Reference yield:

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 132402-59-6
2(S)--3-phenylpropanimino ethyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: NaOH / tetrahydrofuran; H₂O / 18 h / Ambient temperature

2: 1.) N-methylmorpholine, isobutyl chloroformate, 2.) NH₃ / 1) CH₂Cl₂, , -20 deg C, 30 min; 2) CH₂Cl₂, -20 deg C, 15 min, -20 deg C --> rt, 1 h

3: 98 percent / CH₂Cl₂ / 18 h / Ambient temperature

With 4-methyl-morpholine; sodium hydroxide; ammonia; isobutyl chloroformate; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/jo9613491