N²-tert-butyloxycarbonyl-N¹-[6-(2,3,4-tri-O-benzyl-α-L-fucopyranosyloxy)hexyl]-N⁵-[6-(2,4,6-tri-O-benzyl-3-O-p-methoxybenzyl-β-D-galactopyranosyl)hexyl]-L-glutamin-α-amide

Base Information

• Chemical Name: N²-tert-butyloxycarbonyl-N¹-[6-(2,3,4-tri-O-benzyl-α-L-fucopyranosyloxy)hexyl]-N⁵-[6-(2,4,6-tri-O-benzyl-3-O-p-methoxybenzyl-β-D-galactopyranosyl)hexyl]-L-glutamin-α-amide
• CAS No.: 167016-08-2
• Molecular Formula: C₈₄H₁₀₇N₃O₁₆
• Molecular Weight: 1414.78

Synonyms:N²-tert-butyloxycarbonyl-N¹-[6-(2,3,4-tri-O-benzyl-α-L-fucopyranosyloxy)hexyl]-N⁵-[6-(2,4,6-tri-O-benzyl-3-O-p-methoxybenzyl-β-D-galactopyranosyl)hexyl]-L-glutamin-α-amide

Chemical Property of N²-tert-butyloxycarbonyl-N¹-[6-(2,3,4-tri-O-benzyl-α-L-fucopyranosyloxy)hexyl]-N⁵-[6-(2,4,6-tri-O-benzyl-3-O-p-methoxybenzyl-β-D-galactopyranosyl)hexyl]-L-glutamin-α-amide

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Technology Process of N²-tert-butyloxycarbonyl-N¹-[6-(2,3,4-tri-O-benzyl-α-L-fucopyranosyloxy)hexyl]-N⁵-[6-(2,4,6-tri-O-benzyl-3-O-p-methoxybenzyl-β-D-galactopyranosyl)hexyl]-L-glutamin-α-amide

There total 1 articles about N²-tert-butyloxycarbonyl-N¹-[6-(2,3,4-tri-O-benzyl-α-L-fucopyranosyloxy)hexyl]-N⁵-[6-(2,4,6-tri-O-benzyl-3-O-p-methoxybenzyl-β-D-galactopyranosyl)hexyl]-L-glutamin-α-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N2-tert-butyloxycarbonyl-N3-[1-(2,3,4-tri-O-benzyl-α-L-fucopyranosyloxy)-hexyl-6-amino]-L-glutamate-α-amide (167016-51-5) + 6-[(2R,3R,4S,5S,6R)-3,5-Bis-benzyloxy-6-benzyloxymethyl-4-(4-methoxy-benzyloxy)-tetrahydro-pyran-2-yloxy]-hexylamine; compound with toluene-4-sulfonic acid → N2-tert-butyloxycarbonyl-N1-[6-(2,3,4-tri-O-benzyl-α-L-fucopyranosyloxy)hexyl]-N5-[6-(2,4,6-tri-O-benzyl-3-O-p-methoxybenzyl-β-D-galactopyranosyl)hexyl]-L-glutamin-α-amide (167016-08-2)

Guidance literature:

With 1-hydroxy-pyrrolidine-2,5-dione; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃; for 12h;

DOI:10.1248/cpb.47.1237

Reference yield: 72.0%

N2-tert-butyloxycarbonyl-N1-[6-(2,3,4-tri-O-benzyl-α-L-fucopyranosyloxy)hexyl]-N5-[6-(2,4,6-tri-O-benzyl-3-O-p-methoxybenzyl-β-D-galactopyranosyl)hexyl]-L-glutamin-α-amide (167016-08-2) → N2-tert-butyloxycarbonyl-N1-[6-(2,3,4-tri-O-benzyl-α-L-fucopyranosyloxy)hexyl]-N5-[6-(2,4,6-tri-O-benzyl-β-D-galactopyranosyl)hexyl]-L-glutamin-α-amide

Guidance literature:

With water; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 0.5h;

DOI:10.1248/cpb.47.1237

upstream raw materials:

N²-tert-butyloxycarbonyl-N³-[1-(2,3,4-tri-O-benzyl-α-L-fucopyranosyloxy)-hexyl-6-amino]-L-glutamate-α-amide

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