4-acetylphenyl sulfurofluoridate

Base Information

Chemical Name:4-acetylphenyl sulfurofluoridate
CAS No.:133042-62-3
Molecular Formula:C₈H₇FO₄S
Molecular Weight:218.206
Hs Code.:

Synonyms:4-acetylphenyl sulfurofluoridate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-acetylphenyl sulfurofluoridate

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Technology Process of 4-acetylphenyl sulfurofluoridate

There total 1 articles about 4-acetylphenyl sulfurofluoridate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 99-93-4
4-Hydroxyacetophenone

: 133042-62-3
4-acetylphenyl sulfurofluoridate

Guidance literature:: With fluorosulfonyl anhydride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at -78 ℃; for 0.5h;
DOI:10.1021/jo00011a010

Reference yield: 96.0%

: 1809-19-4
dibutyl hydrogen phosphite

: 133042-62-3
4-acetylphenyl sulfurofluoridate

: dibutyl (4-acetylphenyl)phosphonate

Guidance literature:: With (1,2-dimethoxyethane)dichloronickel(II); triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; zinc; In N,N-dimethyl-formamide; at 100 ℃; for 12h; Reagent/catalyst; Solvent; Temperature; Inert atmosphere;
DOI:10.1002/ejoc.202001485