1-((2-(trimethylsilyl)ethoxy)methyl)-2-(1-((2-(trimethylsilyl)ethoxy)methyl)-5-formyl-4-p-tolyl-1H-imidazol-2-yl)-4-p-tolyl-1H-imidazole-5-carbaldehyde

Base Information

Chemical Name:1-((2-(trimethylsilyl)ethoxy)methyl)-2-(1-((2-(trimethylsilyl)ethoxy)methyl)-5-formyl-4-p-tolyl-1H-imidazol-2-yl)-4-p-tolyl-1H-imidazole-5-carbaldehyde
CAS No.:922504-07-2
Molecular Formula:C₃₄H₄₆N₄O₄Si₂
Molecular Weight:630.935
Hs Code.:

1-((2-(trimethylsilyl)ethoxy)methyl)-2-(1-((2-(trimethylsilyl)ethoxy)methyl)-5-formyl-4-p-tolyl-1H-imidazol-2-yl)-4-p-tolyl-1H-imidazole-5-carbaldehyde

Synonyms:1-((2-(trimethylsilyl)ethoxy)methyl)-2-(1-((2-(trimethylsilyl)ethoxy)methyl)-5-formyl-4-p-tolyl-1H-imidazol-2-yl)-4-p-tolyl-1H-imidazole-5-carbaldehyde

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Chemical Property of 1-((2-(trimethylsilyl)ethoxy)methyl)-2-(1-((2-(trimethylsilyl)ethoxy)methyl)-5-formyl-4-p-tolyl-1H-imidazol-2-yl)-4-p-tolyl-1H-imidazole-5-carbaldehyde

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Technology Process of 1-((2-(trimethylsilyl)ethoxy)methyl)-2-(1-((2-(trimethylsilyl)ethoxy)methyl)-5-formyl-4-p-tolyl-1H-imidazol-2-yl)-4-p-tolyl-1H-imidazole-5-carbaldehyde

There total 1 articles about 1-((2-(trimethylsilyl)ethoxy)methyl)-2-(1-((2-(trimethylsilyl)ethoxy)methyl)-5-formyl-4-p-tolyl-1H-imidazol-2-yl)-4-p-tolyl-1H-imidazole-5-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 5720-05-8
4-methylphenylboronic acid

: 591751-01-8
4,4'-dibromo-1,1'-bis[(trimethylsilyl)ethoxymethyl]-2,2'-biimidazole-5,5'-dicarbaldehyde

: 922504-07-2
1-((2-(trimethylsilyl)ethoxy)methyl)-2-(1-((2-(trimethylsilyl)ethoxy)methyl)-5-formyl-4-p-tolyl-1H-imidazol-2-yl)-4-p-tolyl-1H-imidazole-5-carbaldehyde

Guidance literature:: With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; for 7h; Heating;
DOI:10.1139/V06-068

Reference yield: 78.0%

: 922504-07-2
1-((2-(trimethylsilyl)ethoxy)methyl)-2-(1-((2-(trimethylsilyl)ethoxy)methyl)-5-formyl-4-p-tolyl-1H-imidazol-2-yl)-4-p-tolyl-1H-imidazole-5-carbaldehyde

: 922504-08-3
2-(5-formyl-4-p-tolyl-1H-imidazol-2-yl)-4-p-tolyl-1H-imidazole-5-carbaldehyde

Guidance literature:: With hydrogenchloride; In ethanol; for 1h; Heating;
DOI:10.1139/V06-068

Reference yield:

: 922504-07-2
1-((2-(trimethylsilyl)ethoxy)methyl)-2-(1-((2-(trimethylsilyl)ethoxy)methyl)-5-formyl-4-p-tolyl-1H-imidazol-2-yl)-4-p-tolyl-1H-imidazole-5-carbaldehyde

: 2,7,20,25-tetra(p-methylphenyl)-11,16,29,34-tetraethyl-12,15,30,33-tetramethyl-3,6,21,24-tetraaza[32]octaphyrin(1.0.1.0.1.0.1.0.)

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / HCl / ethanol / 1 h / Heating

2: trifluoroacetic acid / methanol; tetrahydrofuran / 20 °C

With hydrogenchloride; trifluoroacetic acid; In tetrahydrofuran; methanol; ethanol;
DOI:10.1139/V06-068