N-(12-(tert-butyldiphenylsilyloxy)dodec-5(Z)-enyl)-N-isopropyl n-heptanamide

Base Information

Chemical Name:N-(12-(tert-butyldiphenylsilyloxy)dodec-5(Z)-enyl)-N-isopropyl n-heptanamide
CAS No.:1402548-00-8
Molecular Formula:C₃₈H₆₁NO₂Si
Molecular Weight:591.993
Hs Code.:

Synonyms:N-(12-(tert-butyldiphenylsilyloxy)dodec-5(Z)-enyl)-N-isopropyl n-heptanamide

Suppliers and Price of N-(12-(tert-butyldiphenylsilyloxy)dodec-5(Z)-enyl)-N-isopropyl n-heptanamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-(12-(tert-butyldiphenylsilyloxy)dodec-5(Z)-enyl)-N-isopropyl n-heptanamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-(12-(tert-butyldiphenylsilyloxy)dodec-5(Z)-enyl)-N-isopropyl n-heptanamide

There total 7 articles about N-(12-(tert-butyldiphenylsilyloxy)dodec-5(Z)-enyl)-N-isopropyl n-heptanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 111-14-8
oenanthic acid

: 1402547-99-2
1-(tert-butyldiphenylsilyloxy)-12-N-isopropylamino-dodec-7(Z)-ene

: 1402548-00-8
N-(12-(tert-butyldiphenylsilyloxy)dodec-5(Z)-enyl)-N-isopropyl n-heptanamide

Guidance literature:: With dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; for 12h;

Reference yield:

: 622842-63-1
tert-butyldiphenyl-[(12-(tetrahydro-2H-pyran-2-yloxy)dodec-7-ynyloxy)]silane

: 1402548-00-8
N-(12-(tert-butyldiphenylsilyloxy)dodec-5(Z)-enyl)-N-isopropyl n-heptanamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: methanol / toluene-4-sulfonic acid / 10 h / 20 °C

2.1: hydrogen; sodium tetrahydroborate / ethylenediamine; nickel(II) acetate tetrahydrate / ethanol / 1 h

3.1: 1H-imidazole; triphenylphosphine / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere

3.2: 3 h / 20 °C

4.1: potassium carbonate / tetrahydrofuran / 12 h / 90 °C / Sealed tube

5.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 12 h

With 1H-imidazole; methanol; dmap; sodium tetrahydroborate; hydrogen; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triphenylphosphine; nickel(II) acetate tetrahydrate; toluene-4-sulfonic acid; ethylenediamine; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;

Reference yield:

: 1402547-82-3
12-(tert-butyldiphenylsilyloxy)dodec-5-yn-1-ol

: 1402548-00-8
N-(12-(tert-butyldiphenylsilyloxy)dodec-5(Z)-enyl)-N-isopropyl n-heptanamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogen; sodium tetrahydroborate / ethylenediamine; nickel(II) acetate tetrahydrate / ethanol / 1 h

2.1: 1H-imidazole; triphenylphosphine / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere

2.2: 3 h / 20 °C

3.1: potassium carbonate / tetrahydrofuran / 12 h / 90 °C / Sealed tube

4.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 12 h

With 1H-imidazole; dmap; sodium tetrahydroborate; hydrogen; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triphenylphosphine; nickel(II) acetate tetrahydrate; ethylenediamine; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;