2-(4-{4-[1-(6,7,10-trioxa-spiro[4.5]dec-8-yl)-vinyl]-phenoxy}-phenoxy)-ethanol

Base Information

Chemical Name:2-(4-{4-[1-(6,7,10-trioxa-spiro[4.5]dec-8-yl)-vinyl]-phenoxy}-phenoxy)-ethanol
CAS No.:1189339-27-2
Molecular Formula:C₂₃H₂₆O₆
Molecular Weight:398.456
Hs Code.:

Synonyms:2-(4-{4-[1-(6,7,10-trioxa-spiro[4.5]dec-8-yl)-vinyl]-phenoxy}-phenoxy)-ethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(4-{4-[1-(6,7,10-trioxa-spiro[4.5]dec-8-yl)-vinyl]-phenoxy}-phenoxy)-ethanol

Chemical Property:

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Technology Process of 2-(4-{4-[1-(6,7,10-trioxa-spiro[4.5]dec-8-yl)-vinyl]-phenoxy}-phenoxy)-ethanol

There total 7 articles about 2-(4-{4-[1-(6,7,10-trioxa-spiro[4.5]dec-8-yl)-vinyl]-phenoxy}-phenoxy)-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1189339-44-3
3-{4-[4-(2-hydroxy-ethoxy)-phenoxy]-phenyl}-but-2-en-1-ol

: 120-92-3
cyclopentanone

: 1189339-27-2
2-(4-{4-[1-(6,7,10-trioxa-spiro[4.5]dec-8-yl)-vinyl]-phenoxy}-phenoxy)-ethanol

Guidance literature:: With hydrogenchloride; oxygen; methylene blue; In tetrahydrofuran; acetonitrile; at 0 - 20 ℃; for 7h; Irradiation;
DOI:10.1016/j.bmcl.2021.128305

Reference yield:

: 1189339-47-6
C₁₈H₂₀O₆

: 120-92-3
cyclopentanone

: 1189339-27-2
2-(4-{4-[1-(6,7,10-trioxa-spiro[4.5]dec-8-yl)-vinyl]-phenoxy}-phenoxy)-ethanol

Guidance literature:: With hydrogenchloride; In water; acetonitrile; at 20 ℃; for 1h;

Reference yield:

: 403-42-9
1-(4-fluorophenyl)ethanone

: 1189339-27-2
2-(4-{4-[1-(6,7,10-trioxa-spiro[4.5]dec-8-yl)-vinyl]-phenoxy}-phenoxy)-ethanol

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / dimethyl sulfoxide / 4 h / Reflux

2.1: potassium carbonate / acetone / 8 h / Reflux

3.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere

3.2: 20 h / 20 °C / Inert atmosphere

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

5.1: methylene blue; oxygen; hydrogenchloride / tetrahydrofuran; acetonitrile / 7 h / 0 - 20 °C / Irradiation

With hydrogenchloride; lithium aluminium tetrahydride; oxygen; methylene blue; sodium hydride; potassium carbonate; In tetrahydrofuran; dimethyl sulfoxide; acetone; acetonitrile; mineral oil;
DOI:10.1016/j.bmcl.2021.128305