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3,3'-thiodibenzoic acid

Base Information
  • Chemical Name:3,3'-thiodibenzoic acid
  • CAS No.:22452-72-8
  • Molecular Formula:C14H10O4S
  • Molecular Weight:274.297
  • Hs Code.:
3,3'-thiodibenzoic acid

Synonyms:3,3'-thiodibenzoic acid

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Chemical Property of 3,3'-thiodibenzoic acid
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Technology Process of 3,3'-thiodibenzoic acid

There total 2 articles about 3,3'-thiodibenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With copper(ll) sulfate pentahydrate; ethane-1,2-dithiol; potassium hydroxide; In water; N,N-dimethyl-formamide; at 120 ℃; for 18h; Inert atmosphere;
DOI:10.1002/adsc.201400941
Guidance literature:
3-Mercapto-benzoesaeure-methylester, 3-Iod-benzoesaeure-methylester, wfr. K2CO3 u. Kupferbronze, Benzylalkohol, N2, Siedetemp., 5h;
Guidance literature:
With pyridine; phenyltrimethylammonium tribromide; for 24h; Ambient temperature;
DOI:10.1055/s-1990-27033
upstream raw materials:

3-Iodobenzoic acid

Downstream raw materials:

3-[(3-carboxyphenyl)sulfinyl]benzenecarboxylic acid

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