(R)-2-(1-(3,4-dichlorophenyl)-1-phenylbutyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:(R)-2-(1-(3,4-dichlorophenyl)-1-phenylbutyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1338922-79-4
Molecular Formula:C₂₂H₂₇BCl₂O₂
Molecular Weight:405.172
Hs Code.:

Synonyms:(R)-2-(1-(3,4-dichlorophenyl)-1-phenylbutyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Chemical Property of (R)-2-(1-(3,4-dichlorophenyl)-1-phenylbutyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of (R)-2-(1-(3,4-dichlorophenyl)-1-phenylbutyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 3 articles about (R)-2-(1-(3,4-dichlorophenyl)-1-phenylbutyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1338922-78-3
C₁₇H₂₇NO₂

: 401797-02-2
2-(3,4-dichlorophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1338922-79-4
(R)-2-(1-(3,4-dichlorophenyl)-1-phenylbutyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: C₁₇H₂₇NO₂; With sec.-butyllithium; In diethyl ether; hexane; cyclohexane; at -78 ℃; for 0.5h; Inert atmosphere;

2-(3,4-dichlorophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; In diethyl ether; hexane; cyclohexane; toluene; at -78 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol202251p

Reference yield:

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 1338922-79-4
(R)-2-(1-(3,4-dichlorophenyl)-1-phenylbutyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: Multi-step reaction with 2 steps

1.1: diethyl ether / 17 h / 20 °C

2.1: sec.-butyllithium / diethyl ether; hexane; cyclohexane / 0.5 h / -78 °C / Inert atmosphere

2.2: 2 h / -78 °C / Inert atmosphere

With sec.-butyllithium; In diethyl ether; hexane; cyclohexane;
DOI:10.1021/ol202251p

Reference yield:

: 151169-75-4
3,4-dichlophenylboronic acid

: 1338922-79-4
(R)-2-(1-(3,4-dichlorophenyl)-1-phenylbutyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: Multi-step reaction with 2 steps

1.1: diethyl ether / 17 h / 20 °C

2.1: sec.-butyllithium / diethyl ether; hexane; cyclohexane / 0.5 h / -78 °C / Inert atmosphere

2.2: 2 h / -78 °C / Inert atmosphere

With sec.-butyllithium; In diethyl ether; hexane; cyclohexane;
DOI:10.1021/ol202251p