(2S)-3-[2-(4-phenylpyridyl)]-1,2-(N,N'-dibenzyloxycarbonyl)diaminopropane

Base Information

Chemical Name:(2S)-3-[2-(4-phenylpyridyl)]-1,2-(N,N'-dibenzyloxycarbonyl)diaminopropane
CAS No.:945723-48-8
Molecular Formula:C₃₀H₂₉N₃O₄
Molecular Weight:495.578
Hs Code.:

Synonyms:(2S)-3-[2-(4-phenylpyridyl)]-1,2-(N,N'-dibenzyloxycarbonyl)diaminopropane

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Chemical Property of (2S)-3-[2-(4-phenylpyridyl)]-1,2-(N,N'-dibenzyloxycarbonyl)diaminopropane

Chemical Property:

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Technology Process of (2S)-3-[2-(4-phenylpyridyl)]-1,2-(N,N'-dibenzyloxycarbonyl)diaminopropane

There total 2 articles about (2S)-3-[2-(4-phenylpyridyl)]-1,2-(N,N'-dibenzyloxycarbonyl)diaminopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 945723-48-8
(2S)-3-[2-(4-phenylpyridyl)]-1,2-(N,N'-dibenzyloxycarbonyl)diaminopropane

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / aq. NaHCO₃ / 24 h / 20 °C

2: 54 percent / iodine; triphenylphosphane; imidazole / CH₂Cl₂ / 3 h / 0 - 20 °C

3: 45 percent / zinc; dibromoethane; chlorotrimethylsilane / triphenylphosphane; [PdCl₂(PPh₃)2] / dimethylformamide / 12 h / 55 °C

With 1H-imidazole; chloro-trimethyl-silane; 1,1-Dibromoethane; iodine; sodium hydrogencarbonate; triphenylphosphine; zinc; bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.200601420

Reference yield:

: 945723-50-2
(2R)-2,3-(N,N'-dibenzyloxycarbonyl)diaminopropanol

: 945723-48-8
(2S)-3-[2-(4-phenylpyridyl)]-1,2-(N,N'-dibenzyloxycarbonyl)diaminopropane

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / iodine; triphenylphosphane; imidazole / CH₂Cl₂ / 3 h / 0 - 20 °C

2: 45 percent / zinc; dibromoethane; chlorotrimethylsilane / triphenylphosphane; [PdCl₂(PPh₃)2] / dimethylformamide / 12 h / 55 °C

With 1H-imidazole; chloro-trimethyl-silane; 1,1-Dibromoethane; iodine; triphenylphosphine; zinc; bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.200601420