Technology Process of W(C5H5)[C5H4(C6F5)]HI
There total 1 articles about W(C5H5)[C5H4(C6F5)]HI which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
tetrahydrofuran;
under N2; adding IC6F5 to THF soln. of WCp2(C2H4), stirring at room temp. for 30 min; filtration under N2, removal of solvent in vacuo, washing residue with hexane, recrystn. from benzene/hexane; elem. anal.;
DOI:10.1021/ja003339u
- Guidance literature:
-
In
dichloromethane;
dissolving W complex in CH2Cl2 in the open, adding CHI3, stirring for 1 h; filtration, redn. of solvent vol. under reduced pressure, addn. of hexane, recrystn. from CH2Cl2/hexane, washing with EtOH then hexane; elem. anal.;
DOI:10.1021/ja003339u
- Guidance literature:
-
With
air;
In
not given;
exposure of soln. of the complex to air; isoln. of product from soln.;
DOI:10.1021/ja003339u
![[W(η-C5H5)2(η-ethylene)]](/Databaselist/images/loading.webp)
