3β,17α-dihydroxy-16β-[(O-β-D-xylopyranosyl-(1→3)-α-L-arabinopyranosyl)oxy]cholest-5-en-22-one

Base Information

• Chemical Name: 3β,17α-dihydroxy-16β-[(O-β-D-xylopyranosyl-(1→3)-α-L-arabinopyranosyl)oxy]cholest-5-en-22-one
• CAS No.: 145075-83-8
• Molecular Formula: C₃₇H₆₀O₁₂
• Molecular Weight: 696.876
• Mol file: 145075-83-8.mol

Synonyms:3β,17α-dihydroxy-16β-[(O-β-D-xylopyranosyl-(1→3)-α-L-arabinopyranosyl)oxy]cholest-5-en-22-one

Chemical Property of 3β,17α-dihydroxy-16β-[(O-β-D-xylopyranosyl-(1→3)-α-L-arabinopyranosyl)oxy]cholest-5-en-22-one

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3β,17α-dihydroxy-16β-[(O-β-D-xylopyranosyl-(1→3)-α-L-arabinopyranosyl)oxy]cholest-5-en-22-one

There total 2 articles about 3β,17α-dihydroxy-16β-[(O-β-D-xylopyranosyl-(1→3)-α-L-arabinopyranosyl)oxy]cholest-5-en-22-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3β,16β,17α-trihydroxycholest-5-en-22-one 16-O-{O-[2-O-(4-methoxybenzoyl)-β-D-xylopyranosyl]-(1->3)-2-O-acetyl-β-L-arabinopyranoside} (145075-81-6) → 4-methoxybenzoic acid (100-09-4) + 3β,17α-dihydroxy-16β-[(O-β-D-xylopyranosyl-(1→3)-α-L-arabinopyranosyl)oxy]cholest-5-en-22-one (145075-83-8)

Guidance literature:

With potassium hydroxide; In ethanol; for 1h; Ambient temperature;

DOI:10.1016/S0031-9422(00)97565-4

Reference yield:

3β,17α-dihydroxy-16β-[[O-(2-O-(3,4-dimethoxybenzoyl)-β-D-xylopyranosyl)-(1→3) -2-O-acetyl-α-L-arabinopyranosyl]oxy]cholest-5-en-22-one → Veratric acid (93-07-2) + 3β,17α-dihydroxy-16β-[(O-β-D-xylopyranosyl-(1→3)-α-L-arabinopyranosyl)oxy]cholest-5-en-22-one (145075-83-8)

Guidance literature:

With potassium hydroxide; In ethanol; for 1h; Ambient temperature;

DOI:10.1016/S0031-9422(00)97565-4

upstream raw materials:

3β,16β,17α-trihydroxycholest-5-en-22-one 16-O-{O-[2-O-(4-methoxybenzoyl)-β-D-xylopyranosyl]-(1->3)-2-O-acetyl-β-L-arabinopyranoside}