C₈₆H₉₄O₁₂S₈

Base Information

• Chemical Name: C₈₆H₉₄O₁₂S₈
• CAS No.: 836605-40-4
• Molecular Formula: C₈₆H₉₄O₁₂S₈
• Molecular Weight: 1576.21
• Mol file: 836605-40-4.mol

Synonyms:C₈₆H₉₄O₁₂S₈

Chemical Property of C₈₆H₉₄O₁₂S₈

Chemical Property:

Purity/Quality:

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Technology Process of C₈₆H₉₄O₁₂S₈

There total 1 articles about C₈₆H₉₄O₁₂S₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

5-(2-{4-[2-(5-hydroxynaphthalen-1-yl)ethynyl]phenyl}ethynyl)naphthalen-1-ol (861885-26-9) + Toluene-4-sulfonic acid 2-[2-((E)-4'-{2-[2-(2,6-diisopropyl-phenoxy)-ethoxy]-ethoxymethyl}-[2,2']bi[[1,3]dithiolylidene]-4-ylmethoxy)-ethoxy]-ethyl ester (861885-25-8) → C86H94O12S8 (836605-40-4)

Guidance literature:

With 18-crown-6 ether; potassium carbonate; lithium bromide; In acetonitrile; for 16h; Heating;

DOI:10.1021/ja051088p

Reference yield: 25.0%

C86H94O12S8 (836605-40-4) + 1,4-bis(bromomethyl)benzene (623-24-5) + 1,1-[1,4-phenylenebis(methylene)]bis-4,4'-pyridylpiridinium bis(hexafluorophosphate) (108861-20-7) → C86H94O12S8*C36H32N4(4+)*4F6P(1-) + C86H94O12S8*2C36H32N4(4+)*8F6P(1-)

Guidance literature:

In N,N-dimethyl-formamide; at 20 ℃; for 168h;

DOI:10.1021/ja051088p

Reference yield: 14.0%

C39H40N4O4S2(2+)*2F6P(1-) + C86H94O12S8 (836605-40-4) + 1,4-bis(bromomethyl)benzene (623-24-5) → C86H94O12S8*C47H48N4O4S2(4+)*4F6P(1-) + C86H94O12S8*2C47H48N4O4S2(4+)*8F6P(1-)

Guidance literature:

With ammonium hexafluorophosphate; In N,N-dimethyl-formamide; at 20 ℃; for 168h; under 9000720 Torr;

DOI:10.1021/ja051088p

upstream raw materials:

5-(2-{4-[2-(5-hydroxynaphthalen-1-yl)ethynyl]phenyl}ethynyl)naphthalen-1-ol

Toluene-4-sulfonic acid 2-[2-((E)-4'-{2-[2-(2,6-diisopropyl-phenoxy)-ethoxy]-ethoxymethyl}-[2,2']bi[[1,3]dithiolylidene]-4-ylmethoxy)-ethoxy]-ethyl ester